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| 1 | 西准达尔布特蛇绿岩中辉长岩LA-ICP-MS锆石U-Pb测年显示文摘达尔布特蛇绿岩中辉长岩LA-ICPMS锆石U-Pb测年,16个测点在谐和曲线图^(206)Pb/^(238)U-^(207)Pb/^(235)U中构成比较集中的锆石群,获得^(206)Pb/^(238)U加权平均年龄391.1±6.8Ma,MSWD=0.97(95%置信度),代表了辉长岩的结晶年龄,据此确定达尔布特蛇绿岩形成于中泥盆世,该年龄的确认为准确约束达尔布特蛇绿岩的形成及西准噶尔板块构造演化提供了重要的佐证。 | 辜平阳 李永军 张兵 佟丽莉 王军年 | 2009 | 岩石学报2009，25，6： | 111 |
| 2 | 宁芜盆地闪长玢岩的形成时代及对成矿的指示意义显示文摘宁芜盆地是长江中下游成矿带的重要组成部分和玢岩型铁矿床的主要产地,盆地内广泛产出闪长玢岩,这类岩体与铁矿床的形成关系密切,但其精确的成岩成矿时代及其形成构造背景的研究仍十分薄弱。本次工作在详细野外地质工作的基础上,系统开展了盆地内与铁矿床有关的7个闪长玢岩体的年代学研究,通过对闪长玢岩锆石LA-ICP-MS同位素定年方法,确定了盆地内主要闪长玢岩体,凹山岩体、陶村岩体、和尚桥岩体、东山岩体、白象山岩体、和睦山岩体和姑山岩体的成岩时代分别为130.2±2.0Ma、130.7±1.8Ma、131.1±1.5Ma、131.1±3.1Ma、130.0±1.4Ma、131.1±1.9Ma和129.2±1.7Ma。定年结果表明盆地内闪长玢岩成岩年龄均为130Ma左右,其成岩年龄可以近似代表铁矿床的成矿年龄。长江中下游地区存在145~136Ma、135~127Ma、126~123Ma三期成岩(成矿)作用,宁芜盆地内闪长玢岩是第二期岩浆活动的产物,其形成时代明显晚于长江中下游成矿带断隆区内与斑岩型-矽卡岩型铜(铁)、金矿床有关的高钾钙碱性岩体。宁芜盆地内闪长玢岩及玢岩型铁矿床形成于区域岩石圈伸展构造环境。 | 范裕 周涛发 袁峰 张乐骏 钱兵 马良 David RC | 2010 | 岩石学报2010，26，9： | 94 |
| 3 | 小兴安岭西北部石炭纪地层火山岩的锆石LA-ICP-MSU-Pb年代学及其地质意义显示文摘小兴安岭西北部晚古生代火山-沉积地层时代的厘定对讨论区域构造演化具有重要意义。本文对该区晚古生代火山岩和粉砂岩进行了锆石LA-ICP-MSU-Pb年代学研究。结果表明,原晚石炭世-早二叠世宝力高庙组、早二叠世大石寨组和晚二叠世五道岭组火山岩均形成于石炭纪,锆石U-Pb年龄集中于353~352Ma和307~306Ma。早石炭世洪湖吐河组上部粉砂岩的碎屑锆石具有两组206Pb/238U谐和年龄,其加权平均年龄分别为385.2±6Ma和353.0±3.6Ma,前者与区域中晚泥盆世钙碱性火山岩的时代相近,后者与早石炭世火山岩的年龄一致,表明沉积物源主要来自中晚泥盆世-早石炭世火山岩,沉积上限为杜内期。新的年代学资料及地层学资料表明,区域早石炭世火山活动(353~352Ma)伴有洪湖吐河组海相沉积,晚石炭世火山活动(307~306Ma)则伴有宝力高庙组陆相沉积。综合区域上普遍缺失巴什基尔阶,认为大兴安岭北部-小兴安岭西北部地区早石炭世晚期发生的海-陆转变与额尔古纳-兴安地块和松嫩地块的碰撞拼合密切相关,早石炭世火山岩可能形成于碰撞前的俯冲环境,晚石炭世火山岩形成于碰撞后的伸展背景。 | 赵芝 迟效国 潘世语 刘建峰 孙巍 胡兆初 | 2010 | 岩石学报2010，26，8： | 89 |
| 4 | Genesis of zircon and its constraints on interpretation of U-Pb age显示文摘Zircon U-Pb dating is the most commonly used method for isotopic geochronology. However, it has been a difficult issue when relating zircon U-Pb ages to metamor- phic conditions in complex metamorphic rocks. Much pro- gress has been made in the past decade with respect to the genesis of zircon and its constraints on interpretation of U-Pb age. Three methods have been proposed to link zircon U-Pb age to metamorphic conditions: (ⅰ) internal structure; (ⅱ) trace element feature; (ⅲ) mineral inclusion composition. Magmatic zircon shows typical oscillatory zoning and/or sector zoning, whereas metamorphic zircon has internal structures such as no zoned, weakly zoned, cloudy zoned, sector zoned, planar zoned, and patched zoned ones. Zircons formed in different geological environments generally have characteristic internal structures. Magmatic zircons from different rock types have variable trace element abundances, with a general trend of increasing trace element abundances in zircons from ultramafic through mafic to granitic rocks. Zircons formed under different metamorphic conditions have different trace element characteristics that can be used to relate their formation to metamorphic conditions. It is an effective way to relate zircon growth to certain P-T condi- tions by studying the trace element partitioning between coexisting metamorphic zircon and garnet in high-grade metamorphic rocks containing both zircon and garnet. Pri- mary mineral inclusions in zircon can also provide unambi- guous constraints on its formation conditions. Therefore, interpretation of zircon U-Pb ages can be constrained by its internal structure, trace element composition, mineral inclu- sion and so on. | WUYuanbao ZHENGYongfei | 2004 | Chinese Science Bulletin2004，49，15： | 723 |
| 5 | 湘东南黄沙坪花岗岩LA-ICPMS锆石U-Pb定年及岩石地球化学特征显示文摘湘东南花岗岩带位于南岭花岗岩带中段,包含以千里山、骑田岭等为代表的花岗岩类和以水口山、铜山岭及宝山为代表的花岗闪长岩类。黄沙坪花岗岩体与前者相邻产出,在岩石地球化学上也具有相类似的特征,其主量元素表现为高硅、高钾、高K2O/Na2O比值,低磷,微量元素以富集Rb、Th、U、K、Ta、Nb,贫Ba、Sr、P、Eu、Ti为特征,具有明显的Eu负异常。利用LA-ICP-MS锆石U-Pb原位定年方法,测得黄沙坪花岗岩的年龄为161.6±1.1Ma,也与区内千里山(162.55±3.25Ma)、骑田岭(161±2Ma)等花岗岩岩体的年龄基本一致,代表了湘东南乃至南岭地区燕山期花岗岩的主要形成时期。因此本文认为,黄沙坪花岗岩体与千里山、骑田岭等岩体属于同一类型,岩石成因可能与印支造山运动后的岩石圈伸展有关,形成于地壳物质的部分熔融;而与水口山、铜山岭和宝山等花岗闪长质岩体有较明显差异。 | 姚军明 华仁民 林锦富 | 2005 | 岩石学报2005，21，3： | 94 |
| 6 | Emplacement age of the Tahe granite and its constraints on the tectonic nature of the Ergun block in the northern part of the Da Hinggan Range显示文摘Large-scale granitic plutons are exposed in the Ergun block in the northern part of the Da Hinggan Range, but their emplacement age and petrogenesis remain un-known. Of these plutons, the Tahe pluton is composed mainly of porphyritic syenogranite and monzogranite, with minor hornblende alkali feldspar granite and gabbro, which have affinities to post-orogenic granitoids. Laser-ablation Induc-tively Coupled Plasma Mass-spectroscope (LA-ICP-MS) analysis shows that the major rock types of the Tahe pluton formed at 494-480 Ma ago, indicating its emplacement in the Early Paleozoic. It is concluded, therefore, that the colli-sion between the Ergun and the Xing’an blocks ended in Early Paleozoic. Considering the geochronological data of the plutons in the adjacent areas, the Early Paleozoic evolu-tionary history of the Ergun block is similar to the central Mongolia and the Tuvino blocks in Mongolia, and the Ergun block should be a part of the accretionary continental mar-gin in the southern Siberian Craton. | GE Wenchun WU Fuyuan ZHOU Changyong Abdel Rahman A. A. | 2005 | Chinese Science Bulletin2005，50，18： | 111 |
| 7 | 辽西东南部中生代花岗岩时代显示文摘辽西东南部是华北地台中生代花岗质岩浆作用较为发育的地区,并产有著名的杨家杖子钼矿床。但关于该区花岗岩的形成时代,一直缺乏深入的研究。本文通过细致的野外考察和系统采样,对该区不同类型的花岗质岩石进行了锆石U- Pb同位素测年。结果显示,该区的碱厂-杨家杖子岩体主体形成于180~190 Ma,部分岩石形成于150~160 Ma左右。东部海棠山-医巫闾山岩体主要形成于150~170 Ma左右。因此,该区的中生代花岗质岩浆作用主要发生在侏罗纪,而白垩纪花岗质岩浆作用相对较弱。同时。这些年代学资料还反映,区内的杨家杖子钼矿形成于中侏罗世,其东部的瓦子峪变质核杂岩形成于早白垩世。对比整个燕辽地区中生代岩浆作用的年代资料发现,该区中生代花岗岩且有自东向西逐渐年轻的趋势,且与火山作用的年代学格架有所不同。岩石中含有的捕获的古老锆石还表明,区内的早前寒武纪岩浆作用主要发生在25和18.5亿年左右。 | 吴福元 杨进辉 张艳斌 柳小明 | 2006 | 岩石学报2006，22，2： | 118 |
| 8 | 黑龙江省东部饶河杂岩的就位时代与东北东部中生代构造演化显示文摘黑龙江省东部饶河杂岩由含放射虫深海沉积岩以及镁铁质的熔岩和侵入岩组成,并被视为大洋壳的残片。该杂岩被晚期蛤蚂河和太平村花岗岩侵入。锆石U-Pb年龄结果表明,上述两花岗岩岩体均形成于早白垩世,其中蛤蚂河岩体形成于131、124和~115Ma三个阶段,太平村岩体形成于111~114Ma左右。饶河杂岩中辉长岩的锆石U-Pb年龄为166±1Ma,深海沉积岩中最晚出现的放射虫的时代为160~150Ma,显示饶河杂岩的就位应发生在150~131Ma的晚侏罗世—早白垩世,古地磁资料显示本区自晚三叠世—侏罗纪有明显的从低纬度向高纬度的北移现象:从而表明在晚侏罗世—早白垩世及以前该区存在太平洋板块的俯冲-走滑作用。岩石学研究显示,两花岗岩岩体中均存在岩浆结晶成因的堇青石,并具有过铝质花岗岩的特点,为典型的来源于沉积岩部分熔融形成的S型花岗岩。Hf同位素测定发现,这些花岗岩中的锆石具有较高的^(176) Hf/^(177)Hf同位素比值和较正的ε_(Hf)(t)值,以长英质地壳为源岩的Hf同位素模式年龄为500~780Ma,说明其源岩应为新元古代—显生宙新增生的地壳物质,从而反映在晚侏罗世—早白垩世以前本区曾发生过显著的地壳抬升与风化剥蚀。 | 程瑞玉 吴福元 葛文春 孙德有 柳小明 杨进辉 | 2006 | 岩石学报2006，22，2： | 84 |
| 9 | 南岭西段花山-姑婆山侵入岩带锆石U-Pb年龄格架及其地质意义显示文摘花山-姑婆山侵入岩带位于南岭西段,由牛庙、同安、花山、金子岭、乌羊山和姑婆山等岩体所组成,10个锆石样品的 SHRIMP U-Pb 法、LA-ICP-MS 法和熔融法定年结果显示,该带中主要的闪长质和花岗质岩体侵位于160~163Ma 这一狭窄的时间范围内,表明中—晚侏罗世之交是本区岩浆活动的高峰时期,它们在时间上、空间上、物质来源上、构造背景上和成因机制上有着十分密切的联系。姑婆山里松花岗岩与其中暗色包体结晶年龄的一致性,从一个重要的方面否定了暗色包体是浅部围岩捕虏体或深部熔融残留体的可能性,并为它们的岩浆混合成因提供了一个重要依据。具有充分分异演化特征的新路晚阶段细粒花岗岩小岩体中锆石的 U-Pb 年龄值为151Ma,比主体花岗岩大约晚10Ma,它可能反映了本区主体花岗岩岩浆房分离结晶和演化的时间跨度。桂岭和大宁岩体侵位于加里东晚期。 | 朱金初 张佩华 谢才富 张辉 杨策 | 2006 | 岩石学报2006，22，9： | 85 |
| 10 | 冀北承德盆地髫髻山组火山岩的时代显示文摘随着近年来的研究进展,代表燕山期大规模火山喷发的髫髻山期(蓝旗期)火山岩的年代学数据得到迅速积累。本文在结合前人对燕山地区髫髻山期(蓝旗期)火山岩 U-Pb 同位素定年工作的基础上,对取自冀北承德盆地兴隆山附近髫髻山组火山岩顶、底样品的锆石进行 U-Pb LA-ICP-MS 定年,试图进一步限定该地区髫髻山期火山岩起始和结束的时代。承德盆地髫髻山组火山岩定年结果表明,其顶部晶屑凝灰岩时代为153±1Ma(2σ),底部粗安岩时代为156±3Ma(2σ)。两者时代在误差范围内一致,说明该地区髫髻山组火山岩喷发是在短时期内完成的。燕山地区髫髻山期(蓝旗期)火山岩时代综合对比分析结果表明髫髻山组(蓝旗组)火山岩初步限定的底部年龄和顶部年龄分别为158±1Ma、153±1Ma。其形成时代在晚侏罗世。土城子组(后城组)与髫髻山组(蓝旗组)火山岩的界线年龄为153±1Ma,这是第一次获得我国中生代陆相地层界线年龄。土城子组顶部的时限确定在134±2~136±2Ma 之间。其沉积时代为晚侏罗世至早白垩世。而髫髻山组火山岩之下的九龙山组的时代可能亦为晚侏罗世。区域张家口组的底部时代限定在134±2Ma。 | 刘健 赵越 柳小明 | 2006 | 岩石学报2006，22，11： | 83 |
| 11 | Simultaneous in-situ determination of U-Pb age and trace elements in zircon by LA-ICP-MS in 20 μm spot size显示文摘Simultaneous in-situ determination of U-Pb ages and 20 trace elements of three international zircon standards(91500,GJ1 and TEMORA 1) and one laboratory zircon standard(SK10-2) separated from Cenozoic fine-grained gabbro was carried out on quadrupole ICP-MS equipped with 193 nm excimer laser in 20 μm spot size. The weighted mean 206Pb/238U ages of 91500,GJ1 and TEMORA 1 are 1064.4±4.8 Ma(2σ ),603.2±2.4 Ma(2σ ) and 418.2±2.4 Ma(2σ ),respectively. The relative standard de-viations(RSDs) of 206Pb/238U ages(2σ ) are less than 2.2% for single measurements and 0.6% for weighted means. The obtained weighted mean 206Pb/238U ages of three standard zircons agree with the recommended values within 2σ error. The weighted mean 206Pb/238U age of SK10-2 is 31.42±0.25 Ma(2σ ) and the RSDs of 206Pb/238U ages(2σ ) are between 2.4% and 5.7% for single measurements and less than 0.8% for weighted mean. The obtained weighted mean 206Pb/238U age is in good agreement with the age obtained by Yuan(2004). Trace element concentrations of NIST612 and NIST614 obtained under the same LA-ICP-MS operating conditions agree with the recommended values within analytical error. The results indicate that it is possible to measure U-Pb age and trace elements simultaneously by LA-ICP-MS in a small spot size of 20 μm. | LIU XiaoMing GAO Shan DIWU ChunRong YUAN HongLin HU ZhaoChu | 2007 | Chinese Science Bulletin2007，52，9： | 107 |
| 12 | 大兴安岭东北部早古生代花岗岩锆石U-Pb年龄、Hf同位素特征及地质意义显示文摘大兴安岭东北部早古生代花岗岩属于Ⅰ型花岗岩。锆石的LA-ICPMS U-Pb年代学研究表明,十八站岩体、内河岩体、白银纳岩体的形成年龄分别为499±1、500±1和460±1Ma,而查拉班河岩体为一多次侵入的杂岩体,其形成年龄在465~481Ma。结合本区和邻区其它早古生代花岗岩体的锆石U-Pb年龄,限定了大兴安岭东北部地区早古生代花岗岩浆活动的时限为460~500Ma。锆石的LA-MC-ICPMS Hf同位素研究显示,本区早古生代花岗岩的锆石ε_(Hf)(t)多数介于+1.5~+3.8之间,二阶段模式年龄介于1.1~1.4Ga,表明其主要起源于中-新元古代增生的地壳物质。结合兴安地块其它花岗岩的锆石Hf同位素资料,认为额尔古纳地块在中-新元古代时期曾发生一次重要的地壳增生事件,与兴安地块主要为显生宙地壳的特点明显不同。 | 葛文春 隋振民 吴福元 张吉衡 徐学纯 程瑞玉 | 2007 | 岩石学报2007，23，2： | 185 |
| 13 | 大兴安岭东北部侏罗纪花岗质岩石的锆石U-Pb年龄、地球化学特征及成因显示文摘大兴安岭东北部花岗岩锆石的LA-ICPMS U-Pb年龄测定结果表明,前人划分的元古代、早古生代和晚古生代的花岗岩有相当一部分是侏罗纪花岗岩。根据时间先后关系,可将本区侏罗纪花岗岩的侵位顺序划分为早、晚两期,其锆石U-Pb年龄分别为188~190Ma和171~181Ma,这些侏罗纪花岗岩的年龄数据与东北其它地区侏罗纪花岗岩完全可以对比。在地球化学特征上可以将这些花岗质岩石划分为低Sr高Yb型和高Sr低Yb型两类,它们有相同或相似的源岩组成而起源的深度不同,早期侵入的花岗岩为低Sr高Yb型,起源于压力较低的中地壳,而晚期侵入的花岗岩为高Sr低Yb型,类似于'C'型埃达克岩,起源于压力较高的下地壳。锆石Hf同位素成分特征表明,侏罗纪花岗岩的源区物质主要为新元古代和显生宙期间增生的地壳物质及两期增生地壳物质的混合物。本区侏罗纪花岗岩以花岗闪长岩-二长花岗岩为主,为准铝质或弱过铝质、高钾钙碱性系列的Ⅰ型花岗岩,具有类似于活动大陆边缘花岗岩的岩石组合特征,属于呈北北东向带状展布的中国东北地区侏罗纪花岗岩带的一部分,其形成与古太平洋板块的俯冲作用有关。 | 隋振民 葛文春 吴福元 张吉衡 徐学纯 程瑞玉 | 2007 | 岩石学报2007，23，2： | 164 |
| 14 | In situ simultaneous determination of trace elements,U-Pb and Lu-Hf isotopes in zircon and baddeleyite显示文摘This paper describes a combined method of simultaneously measuring U-Pb and Lu-Hf isotopes as well as trace elements in Phalaborwa baddeleyite and 91500, GJ-1, TEMORA-1 and SK10-2 zircons by means of Neptune MC-ICPMS and Agilent Q-ICPMS connected to a 193 nm excimer laser ablation system. Material ablated by laser was carried in different proportions into Q-ICPMS for U-Pb isotopic and trace elemental and MC-ICPMS for Lu-Hf isotopic compositions. Experiments indicate that different proportions of ablated material for the Q-ICPMS and MC-ICPMS (6:4, 5:5 and 4:6 respectively) do not show any bias for the zircon/baddeleyite U-Pb age, Lu-Hf isotope and trace elemental compositions within ana-lytical errors. Using 40―60 μm spot size, the obtained U-Pb ages of Phalaborwa baddeleyite, 91500, GJ-1, TEMORA and SK10-2 zircons are 2065±15 (2σ, n=20), 1063±6 (2σ, n=19), 613±6 (2σ, n=20), 416±5 (2σ, n=20) and 32.6±0.5 (2σ, n=20) Ma, respectively. The 176Hf/177Hf ratios are 0.281231±24 (2SD, n=20), 0.282310±35 (2SD, n=19), 0.282028±34 (2SD, n=20), 0.282687±34 (2SD, n=20) and 0.282752±53 (2SD, n=20), respectively. The obtained trace elemental compositions are identical to the reference values. Therefore, this kind of technique makes it possible to simultaneously obtain the U-Pb age, Lu-Hf iso-topes and trace elemental compositions of zircon and baddeleyite, which could be an important tool in solving problems in earth sciences. | XIE LieWen ZHANG YanBin ZHANG HuiHuang SUN JingFeng WU FuYuan | 2008 | Chinese Science Bulletin2008，53，10： | 97 |
| 15 | 福建北东沿海高分异Ⅰ型花岗岩的成因:锆石U-Pb年代学、地球化学和Nd-Hf同位素制约显示文摘以福建北东沿海的南镇、大层山、三沙和大京四个岩体为对象,系统研究了它们的年代学和地球化学特征,并据此探讨了岩体的成因。锆石LA—ICP—MSU—Pb定年结果表明,南镇、大层山、三沙和大京岩体的成岩年龄分别为96.1±2.7Ma、93.1±2.4Ma、91.5±1.5Ma和93.8±1.8Ma,指示它们均为晚白垩世岩浆活动的产物。这些岩体的组成矿物主要为石英和条纹长石,并含有一定量斜长石(〈15%),铁镁矿物主要为少量黑云母,未出现碱性铁镁矿物,副矿物组合中普遍出现榍石而未见铝过饱和矿物。化学组成上表现为高硅、富碱、准铝,贫钙、镁、铁,Rb/Sr比值高,K/Rb比值低,富Cs、Rb、Th、u、Pb,贫Ba、Sr、P、Ti、Eu。岩石的FeO^*/MgO比值较低(=3.44—5.04),10^4×Ga/Al比值和Zr+Nb+Ce+Y含量均低于A型花岗岩的下限值,其锆石饱和温度也较低(730—779℃),综合地质地球化学特征指示这些岩体应属高分异的Ⅰ型花岗岩。四个岩体的Nd同位素组成较均-(εNd(t)=-4.2~-5.5),而锆石Hf同位素则具较大的变化范围(εHf(t)=-11.6~4.5),εHf(t)值散布于正值与负值之间,变化幅度可达10个εHf单位以上,指示岩体的形成存在不同来源物质的贡献。岩石的形成极可能经历了壳幔物质在源区混合形成原始岩浆,随后这一壳幔混源岩浆又经高程度分异演化的二阶段成岩过程,而并非起源于幔源岩浆底侵形成的初生地壳与古老基底地壳混合的地壳原岩的部分熔融。 | 邱检生 肖娥 胡建 徐夕生 蒋少涌 李真 | 2008 | 岩石学报2008，24，11： | 197 |
| 16 | LA-MC-ICP-MS锆石微区原位U-Pb定年技术显示文摘利用激光多接收等离子体质谱(LA-MC-ICP-MS)技术对30~1065Ma的系列锆石进行了详细的定年研究。包含离子计数器的多接收系统使得不同质量数的同位素信号可以同时静态接收,并且不同质量数的峰基本上都是平坦的,进而可以获得高精度的数据,均匀锆石颗粒207Pb/206Pb、206Pb/238U、207Pb/235U比值的测试精度(2σ)均为2%左右,对锆石标准的定年精度和准确度在1%(2σ)左右;不同质量数同位素信号的同时静态接收使得剥蚀时间缩短,剥蚀深度变浅,相比LA-ICP-MS方法,提高了激光剥蚀的空间分辨率。对5个锆石标准和2个实际样品的测试表明,206Pb/238U年龄测定误差在1%(2σ)以内,定年结果在误差范围内与前人报道值完全一致,测试精度达到国际同类实验室先进水平。 | 侯可军 李延河 田有荣 | 2009 | 矿床地质2009，28，4： | 867 |
| 17 | Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS显示文摘A protocol was established for simultaneous measurements of zircon U-Pb ages and trace elements by LA-ICP-MS at spot sizes of 16 32 μm.This was accomplished by introducing N 2 into ICP to increase the sensitivity.The obtained U-Pb ages for zircon standards GJ-1,TEMORA and SK10-2 are consistent with the preferred values within about 1% uncertainty (2σ) by simple external calibration against zircon standard 91500.Different data reduction softwares could yield different uncertainties for calculation of U-Pb ages.The commercially available program GLITTER4.4 could apply an improper uncertainty calculation strategy,but it may yield artificial high precisions for single analyses.Our trace element analyses indicate that Si is not an ideal internal standard for zircon when calibrated against the NIST glasses.Calibration against the NIST glasses using Si as an internal standard,a systematic deviation of 10% 30% was found for most trace elements including Zr.However,the trace element compositions of zircon can be accurately measured by calibration against multiple reference materials with natural compositions (e.g.,BCR-2G,BHVO-2G and BIR-1G),or calibration against NIST SRM 610 and using Zr as an internal standard.Analyses of two pieces of GJ-1 demonstrate that it is relatively homogenous for most trace elements (except for Ti). | LIU YongSheng HU ZhaoChu ZONG KeQing GAO ChangGui GAO Shan XU Juan CHEN HaiHong | 2010 | Chinese Science Bulletin2010，55，15： | 1011 |
| 18 | 东昆仑南缘阿尼玛卿构造带布青山地区两期蛇绿岩的LA-ICP-MS锆石U-Pb定年及其构造意义显示文摘东昆仑南缘布青山地区是阿尼玛卿蛇绿构造混杂岩带的西延组成部分,由各种不同构造岩片混杂堆积而成。通过对布青山地区得力斯坦沟和哈尔郭勒两处蛇绿岩的详细野外调查、岩石组合研究,对两处蛇绿岩中的辉长岩分别进行了LA-ICP-MS锆石U-Pb定年,得到206Pb/238U加权平均年龄为516.4±6.3Ma(MSWD=0.70)和332.8±3.1Ma(MSWD=0.75),分别代表了两处蛇绿岩中辉长岩的结晶年龄,表明布青山地区存在早寒武世和早石炭世两期蛇绿岩,这两期蛇绿岩的存在代表了布青山-阿尼玛卿构造带古洋盆两次扩张过程中岩浆活动的产物,表明了原特提斯洋与古特提斯洋的形成及其构造演化。 | 刘战庆 裴先治 李瑞保 李佐臣 张晓飞 刘智刚 陈国超 陈有炘 丁仨平 郭俊锋 | 2011 | 地质学报2011，85，2： | 113 |
| 19 | North Qinling Paleozoic granite associations and their variation in space and time: Implications for orogenic processes in the orogens of central China显示文摘Integrated zircon U-Pb dating and whole rock geochemical analyses have been carried out for two typical S-and I-type granitoids in the north Qinling. Zircon dating by SIMS of the Piaochi S-type grani- toids yields an emplacement age of 495±6 Ma. The granitoids show whole-rock εNd(t)=-8.2--8.8, zircon εHf(t)=-6―-39. The Huichizi I-type granitoids have emplacement ages of 421±27 Ma and 434±7 Ma es- tablished by LA-ICP-MS and SIMS methods, respectively. Their whole-rock εNd(t)=-0.9-0.9 and zircon εHf(t)=-11-8.4. Combined with statistical analyses of 28 zircon ages of granitoid plutons collected from the literature, Paleozoic magmatism in the north Qinling can be divided into three stages. The first-stage magmatism (~505-470 Ma) mainly occurred in the east part of the north Qinling and has features of an I-type arc, associated with which are S-type granitoids such as Piaochi pluton. The early granitoids (~505-490 Ma) have close spatio-temporal relations to ultra-high-pressure (UHP) rocks, and thus are interpreted as an oceanic subduction system along a continental margin. The second-stage magmatism (~450-422 Ma) occured through the whole north Qinling, and is characterized by I-type granitoids represented by the Huichizi pluton. The magma is interpreted as partial melting of lower crust mixed by mantle-derived magma in a collisional setting with the uplift of terranes. The third-stage magmatism (~415-400 Ma) is dominated by I-type granitoids and only took place in the middle part of the north Qinling, and is regarded as a late-stage collision. The spatial and temporal variations of the Qinling Paleozoic magmatism reveal protracted subduction/collision. The subduction was initiated from the east part of the north Qinling, earlier than that in the Qilian-northern Qaidam, Kunlun, and northern Dabie regions. This demonstrates variations in time of subduction, accretion and collision of separate blocks or terranes in the orogenic systems in central China. | WANG Tao WANG XiaoXia TIAN Wei ZHANG ChengLi LI WuPing LI Shan | 2009 | Science China Earth Sciences2009，52，9： | 79 |
| 20 | 内蒙古牙克石地区晚古生代弧岩浆岩:年代学及地球化学证据显示文摘在内蒙古牙克石地区晚古生代岩浆岩中发现了岛弧火山岩和埃达克质花岗闪长岩。火山岩由玄武岩、安山岩、英安岩及凝灰岩组成,属于钙碱性系列,它们富集大离子亲石元素(LILE)、轻稀土元素(LREE),亏损高场强元素(HFSE)。玄武岩的SHPIMP锆石U-Pb年龄表明其形成于373.2±5.3Ma。锆石εHf(t)值为+14.67~+18.67,类似大洋中脊玄武岩(MORB)和现代俯冲带玄武岩的Hf同位素特征。上述特征说明,玄武岩很可能起源于受俯冲板片流体改造的亏损地幔楔,形成于活动大陆边缘。花岗闪长岩的结晶年龄为331.2±3.7Ma。岩石高SiO2、Sr,高Sr/Y比值,富集轻稀土元素,亏损重稀土元素和Y及高场强元素,铕异常基本不明显,具备埃达克岩的地球化学特征。锆石εHf(t)值较高(+12.78~+14.54),说明源区可能为亏损地幔或新生的玄武质下地壳。根据微量元素组成认为花岗闪长岩主要起源于晚古生代底侵的岛弧玄武-安山质下地壳。弧火山岩和埃达克质花岗闪长岩的发现表明,区内晚泥盆世-早石炭世发生过大洋板片的俯冲作用,可能与额尔古纳-兴安地块与松嫩地块的碰撞拼合密切相关。 | 赵芝 迟效国 刘建峰 王铁夫 胡兆初 | 2010 | 岩石学报2010，26，11： | 77 |
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