A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride

查看全文 作　　者：Deng, [1]Cheng;Song, Yong [1]Cai;Wang, Ying [1]De;Li, Yi [1]He;Lei, Yong [1]Peng;Cao, Shu [2]Wei

机构地区：[1]Natl Univ Def & Technol, Coll Aerosp & Mat Engn, State Key Lab Adv Ceram Fibers & Composites, Changsha 410073, Hunan, Peoples R China;[2]Aerosp Res Inst Mat & Proc Technol, Beijing 100076, Peoples R China

出　　处：《Chinese Chemical Letters》索引2010年第21卷第2期,共4页

基　　金：the National'863'Program(No.2006AA03A217) for financial support of the research 摘　　要：2,4,6-Trichloroborazine has been recognized as a desirable monomer for the preparation of high-performance boron nitride fibers through polymer derived ceramics route.So a high yield and facile synthesis of 2,4,6-trichloroborazine is essential in practice. Using boron trichloride-dimethylsulfide complex((CH_3)_2S·BCl_3) and ammonium chloride(NH_4Cl) as starting materials and toluene(C_6H_5CH_3) as solvent,the synthesis of 2,4,6-trichloroborazine to give high yield is reported. 关键词：2,4,6-Trichloroborazine Boron trichloride-dimethylsulfide Boron nitride precursor SYNTHESIS

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A facile synthesis of 2,4,6-trichloroborazine from boron trichloride-dimethylsulfide complex and ammonium chloride

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