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Roles of Te and Mn in the two phases of manganite with nominal composition La_(0.6)Sr_(0.1)Te_xMnO_3

查看全文 作  者:LI [1]Yanfeng;JI [1]Denghui;ZHAO [1]Zhiwei;TANG [1]Guide;LIU [1]Shaopeng;ZHANG [1]Yuge;LI [1]Zhuangzhi;HOU [1]Denglu;ZHU [2]Minggang 高影响力作者 机构地区:[1]Department of Physics, Hebei Normal University, Hebei Advanced Thin Films Laboratory, Shijiazhuang 050016, China;[2]Division of Functional Materials Research, Central Iron & Steel Research Institute, Beijing 100081, China高影响力机构 出  处:《Rare Metals》索引2011年第30卷第3期,共9页高影响力期刊 基  金:supported by the Natural Science Foundation of Hebei Province (No. E2011205083);the Key Item Science Foundation of Hebei Province, China (No.10965125D; No.08965108D);the National Natural Science Foundation of China (No.NSF-10774037;No.10074013);the National High Technology Research and Development Program of China (No. 2007AA03Z100) 摘  要:Powder samples with nominal composition La0.6Sr0.1TexMnO3 (x = 0.00, 0.05, 0.10, 0.15, 0.20) were prepared using the sol-gel method with thermal treatment up to 1473 K. On the basis of powder X-ray diffraction (XRD), thermogravimetric and magnetic measurements, it was found that almost all of the Te and a few of the Mn ions were lost from the samples when they were calcined at 1473 K. The reason for the Te loss and a quantitative phase analysis for the samples calcined at 1473 K are discussed in detail. 关 键 词:锰离子 粉末X射线衍射 MN 粉末样品 定量相分析 热处理 凝胶法 XRD
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