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Precipitation behavior of 14H-LPSO structure in Mg–12Gd–2Er–1Zn–0.6Zr Alloy

查看全文 作  者:Kai [1]Wen;Wen-Bo [1]Du;Ke [1]Liu;Zhao-Hui [1]Wang;Shu-Bo [1]Li 高影响力作者 机构地区:[1]College of Materials Science and Engineering, Beijing University of Technology高影响力机构 出  处:《Rare Metals》索引2016年第35卷第5期,共7页高影响力期刊 基  金:financially supported by the Projects of Beijing Municipal Science and Technology Commission (No. Z131100003213019);the Projects of Beijing Municipal Commission of Education (Nos. KM201110005001 and KM201310005001);Beijing Natural Science Foundation (No. 2144043) 摘  要:The microstructures of as-cast and as-solution Mg–12Gd–2Er–1Zn–0.6Zr alloys were investigated by optical microscopy(OM), scanning electron microscopy(SEM), transmission electron microscopy(TEM), highresolution transmission electron microscopy(HRTEM)X-ray diffraction(XRD) and selected-area electron diffraction(SAED) in the present investigation. The results show that the primary eutectic phase Mg_5(Gd, Er, Zn) and some flocculent features are found in the as-cast alloy; the SAED pattern indicates that these flocculent features are the dense areas of stacking faults. The 14H-LPSO structure precipitates in the temperature range of 673–793 K, and the volume fraction of 14H-LPSO structure increases with the extension of heating time; however, there is no precipitation of 14H-LPSO structure when the temperature reaches up to 803 K. In addition, the Mg_5(Gd, Er, Zn) phase dissolves gradually along with the precipitation of 14H-LPSO structure. 关 键 词:铸态合金 结构相 析出行为 扫描电子显微镜 透射电子显微镜 高分辨透射电镜 HRTEM 选区电子衍射
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