Synthesis of CF2H-Containing Oxime Ethers Derivatives from CICF2H,tert-Butyl Nitrile and Indoles

查看全文 作　　者：Xingxing [1]Ma;Hua [1]Huang;Jianke [1]Su;Zhiyi [4]Song;Tamaki [4]Nakano;Qiuling [1,2,3]Song

机构地区：[1]Institute of Next Generation Matter Transformation,College of Materials Science&Engineering,Huaqiao University,668 JimeiBlvd,Xiamen,Fujian 361021,China;[2]Key Laboratory of Molecule Synthesis and Function Discovery,Fujian Province University,College of Chemistry,Fuzhou University,Fuzhou,Fujian 350108,China;[3]State Key Laboratroy of Organometallic Chemistry,Shanghai Institute of Organic Chemistry,Chinese Academy of Sciences,Shanghai 200032,China;[4]Institute for Catalysis(ICAT),Hokkaido University,N 21,W 10,Kita-ku,Sapporo 001-0021,Japan

出　　处：《Chinese Journal of Chemistry》索引2020年第38卷第1期,共6页

基　　金：Financial support from the National Natural Science Founda-tion of China(No.21772046);the Natural Science Foundation of Fujian Province(No.2016J01064)is gratefully acknowledged.We also thank Instrumental Analysis Center of Huaqiao University for analysis support.X.M.thanks the Subsidized Project for Cul-tivating Postgraduates’Innovative Ability in Scientific Research of Huaqiao University. 摘　　要：Summaryof main observation and conclusion A new and intriguing methodology to access various O-difluoromethylation oxime compounds from CICF2H,TBN and indoles is developed under mild reaction conditions.This strategy can suppress N-difluoromethylation of indoles successfully,in which there are two different active species(:CF2and·NO)while indoles are unprotected,featuringsimple operation and radical involvement. 关键词：conditions. INDOLE CONCLUSION

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Synthesis of CF2H-Containing Oxime Ethers Derivatives from CICF2H,tert-Butyl Nitrile and Indoles

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