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Basic deep eutectic solvents as reactant, template and solvents for ultra-fast preparation of transition metal oxide nanomaterials

查看全文 作　　者：Jia [1,2]Chen;Mohammad Chand [1]Ali;Ruirui [3]Liu;Jean Claude [1,2]Munyemana;Zhan [1]Li;Honglin [3]Zhai;Hongdeng [1,2]Qiu 高影响力作者 机构地区：[1]CAS Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province,Lanzhou Institute of Chemical Physics,Chinese Academy of Sciences,Lanzhou 730000.China;[2]University of Chinese Academy of Sciences,Chinese Academy of Sciences,Beijing 100039,China;[3]Department of Chemistry,Lanzhou University,Lanzhou 730000.China高影响力机构 出　　处：《Chinese Chemical Letters》索引2020年第31卷第6期,共4页高影响力期刊 基　　金：supported by the National Natural Science Foundation of China(Nos.21822407,21675164);the CASPresident International Fellowship Initiative(No.2017PC0014)。 摘　　要：Developing a new type of deep eutectic solvents(DESs)is indispensable for expanding their application in various fields.Here,we report a series of new highly basic DESs.FT-IR,quantitative 1 H NMR,MD simulation and physical properties show that these basic liquids are made up of hydroxide acceptor of alkali metal hydroxides in which the hydrogen bonding interactions coordinate the donor.These DESs can be played three roles as new solvents,template and reactant for facile and ultra-fast preparation of transition metal oxide nanomaterials such as NiCo2 O4,MnCo2 O4,NiMn2 O4,CoCu2 O4 and Co3 O4 under mild condition.This work shows one of the low energy-intensive methods for nanomaterial preparation.These initial findings of basic deep eutectic solvents provide a potential applicability around the systematic development of transition metal oxide nanosheets. 关 键 词：Basic deep eutectic solvents Hydrogen-bonding acceptors Hydrogen-bonding donors Transition metal oxide NANOMATERIALS
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