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| 1 | Controllable preparation of γ-alumina nanoparticles with bimodal pore size distribution in membrane dispersion microreactor显示文摘In this paper,we present a new method for preparing γ-alumina nanoparticles with a bimodal pore size distribution by using an efficiently mixing membrane dispersion microreactor.NH4HCO3and AI2(SO4)3.18H2Owere reacted under vigorous mixing to give an ammonium aluminum carbonate hydroxide (AACH)precursor.γ-Alumina was obtained by calcination of AACH at 550℃ for 6h.The effects of NH4HCO3concentration,pH during aging,and reaction temperature were investigated.The mechanism of bimodal pore formation was clarified.The results showed that large pores (10-100nm) were mainly formed in the reactor and during aging,and small pores (0-10nm)were mainly formed during calcination.When the concentration of NH4HCO3was 1.5mol/L,the aging pH was 9.2,and the reaction temperature was 80℃,γ-alumina with a specific surface area of 504.7m^2/g and pore volume of 1.76mL/g was obtained.The average size of the large pores was about 30nm,and the average size of the small pores was about 4nm. | Lufan Yang Mingzhao Guo Fan Zhang Yu Jing Yujun Wang Guangsheng Luo | 2018 | Particuology2018，16，6： | 2 |
| 2 | Quantitative Shear Wave Velocity Measurement on Acoustic Radiation Force Impulse Elastography for Differential Diagnosis between Benign and Malignant Thyroid Nodules: A Meta-analysis显示文摘 | Bo-Ji Liu Dan-Dan Li Hui-Xiong Xu Le-Hang Guo Yi-Feng Zhang Jun-Mei Xu Chang Liu Lin-Na Liu Xiao-Long Li Xiao-Hong Xu Shen Qu Mingzhao Xing | 2015 | Ultrasound in Medicine & Biology2015，，12： | 1 |
| 3 | Novel Terpyridine-bridged Parallel Dication Metallo-bisviologens and Their Supramolecular Complexes显示文摘By utilizing terpyridine-bridged parallel metallo-complexes as dication metallo-bisviologens,herein we present the synthesis and characterization of two novel supramolecular complexes.1-Methylpyridin-1-ium-terpyridine ligands and their metallo-complexes were first designed and synthesized,and the association of methyl-pyridiniums with dibenzo-24-crawn-8 ether(DB24C8)afforded the desired novel complexes through host-guest interactions.The self-assembly behavior of the supramolecular complexes was comprehensively investigated and could be exploited for furtlaer construction of ID to 3D supramolecular infrastructures. | LIU Qianqian GUO Yuan WU Tun CHEN Mingzhao XIE Tingzheng WANG Pingshan | 2019 | Chemical Research in Chinese Universities2019，35，2： | 0 |
| 4 | Application value of Qisexingtai hand diagnostic method in diagnosis of coronary artery disease显示文摘OBJECTIVE:To evaluate the diagnostic efficacy of Qisexingtai hand diagnostic method in the diagnosis of coronary artery disease(CAD).METHODS:This was an investigator-initiated,prospective,multi-center,cross-sectional study.All the participants from three hospitals in China had been diagnosed by both Qisexingtai hand diagnostic method and coronary angiography.We compared the two diagnostic methods to calculate the sensitivity,the specificity,the omission diagnostic rate,the mistaken diagnostic rate and accuracy in order to evaluate the diagnostic efficacy of Qisexingtai hand diagnostic method for CAD.RESULTS:A total of 326 subjects were enrolled,diagnosed by both Qisexingtai hand diagnostic method and coronary angiography.As a result,there were 166 positive cases according to Qisexingtai hand diagnostic method,and 131 positive cases according to coronary angiography.Compared with the results of coronary angiography,the sensitivity of Qisexingtai hand diagnostic method was 80.2%,the specificity was 68.7%,the omission diagnostic rate was 19.8%,the mistaken diagnostic rate was 31.3%,and the accuracy was 73.3%.Area under the receiver operating characteristic curve was estimated as 0.735 for all,and 0.718,0.735,0.783 for the three sub-centers.CONCLUSION:Qisexingtai hand diagnostic method with high accuracy and sensitivity has certain application value in the diagnosis of CAD. | LIU Qian ZHAO Zhupei GUO Hua WANG Shiheng HAO Mingzhao QIN Peijie WANG Liuqing LIU Xuechun ZHANG Fengxia AN Hong LI Yu SHI Xueqin ZHU Tingyu LIU Jianfeng WANG Liying XU Tao ZHANG Limei ZOU Xu | 2022 | Journal of Traditional Chinese Medicine2022，42，5： | 0 |
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