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| 1 | Simultaneous in-situ determination of U-Pb age and trace elements in zircon by LA-ICP-MS in 20 μm spot size显示文摘Simultaneous in-situ determination of U-Pb ages and 20 trace elements of three international zircon standards(91500,GJ1 and TEMORA 1) and one laboratory zircon standard(SK10-2) separated from Cenozoic fine-grained gabbro was carried out on quadrupole ICP-MS equipped with 193 nm excimer laser in 20 μm spot size. The weighted mean 206Pb/238U ages of 91500,GJ1 and TEMORA 1 are 1064.4±4.8 Ma(2σ ),603.2±2.4 Ma(2σ ) and 418.2±2.4 Ma(2σ ),respectively. The relative standard de-viations(RSDs) of 206Pb/238U ages(2σ ) are less than 2.2% for single measurements and 0.6% for weighted means. The obtained weighted mean 206Pb/238U ages of three standard zircons agree with the recommended values within 2σ error. The weighted mean 206Pb/238U age of SK10-2 is 31.42±0.25 Ma(2σ ) and the RSDs of 206Pb/238U ages(2σ ) are between 2.4% and 5.7% for single measurements and less than 0.8% for weighted mean. The obtained weighted mean 206Pb/238U age is in good agreement with the age obtained by Yuan(2004). Trace element concentrations of NIST612 and NIST614 obtained under the same LA-ICP-MS operating conditions agree with the recommended values within analytical error. The results indicate that it is possible to measure U-Pb age and trace elements simultaneously by LA-ICP-MS in a small spot size of 20 μm. | LIU XiaoMing GAO Shan DIWU ChunRong YUAN HongLin HU ZhaoChu | 2007 | Chinese Science Bulletin2007，52，9： | 107 |
| 2 | LA-(MC)-ICPMS U-Pb zircon geochronology and Lu-Hf isotope compositions of the Taihua complex on the southern margin of the North China Craton显示文摘Widely distributed on the southern margin of the North China Craton,the Taihua complex extends roughly in an east-west direction and the relatively complete successions are found in Lushan County,Henan Province.Like many other Archean terranes,the Taihua Complex can be divided into two major lithological units along the Dangze River,namely gneisses series and supracrustal rocks.The former is located on the north side of the river and chiefly composed of TTG gneisses and amphibolites;the latter on the south side of the river is mainly supracrustal rock.Coupled with the previous studies,the results obtained by this study show that the Taihua complex was formed in a large time span from Neoarchean to Palaeoproterozoic.The TTG gneisses and amphibolites are dated at Neoarchean (2794–2752 Ma).The 2.9 Ga and 3.1 Ga zircons in amphibolites could be xenocrysts.In the North China Craton,the 2.8–2.7 Ga old rocks crop out in several areas e.g.western Shandong Province,Jiaodong Peninsula and Lushan area of Henan Province.In addition,2.8–2.7 Ga detrital zircons or xenocryst zircons have been recognized in Huai’an,Fuping,Wutai areas of North China Craton and also reported in the Early Paleozoic diamondiferous kimberlites in Mengyin and Fuxian.All these age results indicate that the 2.8–2.7 Ga rocks may have been developed much broader region than today’s outcrops.Zircon Hf and whole rock Nd isotopes show that the 2.8–2.7 Ga tectono-thermal event represents an important period of crustal growth with minor ancient crust reworked in the North China Craton.However the formation of supracrustal rocks is limited to 2.2–2.0 Ga in the Palaeoproterozoic time,not the Archaean,as previously believed.Combined with the chronological data of aluminium-rich metamorphic rocks (Khondalite series) on the southern margin of the North China Craton and adjacent areas,it is suggested that the above areas have widely developed Paleoproterozoic passive continental margin environment. | DIWU ChunRong SUN Yong LIN CiLuan WANG HongLiang | 2010 | Chinese Science Bulletin2010，55，23： | 72 |
| 3 | U–Pb ages and Hf isotopes for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southwestern margin of the North China Craton显示文摘In situ U-Pb dating and Lu-Hf isotopic analysis were carried out for detrital zircons from quartzite in the Paleoproterozoic Songshan Group on the southern margin of the North China Craton (NCC). The re- sults provide further constraints on the crustal formation and evolution history of NCC. Four 207Pb/206Pb age populations were obtained from 99 analyses, with clusters at ~3.40 Ga, 2.77―2.80 Ga, ~2.50 Ga and 2.34 Ga, respectively. The 3.40 Ga old zircons have similar Hf isotopic compositions to those from Ar- chean rocks in the Jidong and Anshan areas of NCC. However, crustal remnants older than 3.6 Ga have been identified in the southern margin of NCC, the South China Craton, the northwestern part of the Qinling Orogen and its adjacent area. Thus, it is not easy to trace the source rock from which the 3.40 Ga detrital zircons were derived. It can be inferred that the crustal remnants older than 3.40 Ga might have been widely distributed in the North China Craton. The 2.77―2.80 Ga zircons make up a relatively small proportion and have the highest εHf (t) values (up to 6.1±1.6), consistent with the Hf isotopic composition of the depleted mantle at 2.83 Ga. Their single-stage Hf model age of 2.83 Ga is close to their crystallized age, suggesting that their source rocks were extracted from the contemporaneous depleted mantle. The ~2.50 Ga zircon grains constitute about 85% of the total grain population and their Hf isotopic compositions indicate major growth of juvenile crust at ~2.50 Ga but minor reworking of ancient crust. The youngest zircon dated in this study gave an U-Pb age of 2337±23 Ma, which can be considered the maximum depositional age of the formation of the Songshan Group. | DIWU ChunRong SUN Yong YUAN HongLin WANG HongLiang ZHONG XingPing LIU XiaoMing | 2008 | Chinese Science Bulletin2008，53，18： | 54 |
| 4 | Geochronological,geochemical,and Nd-Hf isotopic studies of the Qinling Complex,central China:Implications for the evolutionary history of the North Qinling Orogenic Belt显示文摘The Qinling Complex of central China is thought to be the oldest rock unit and the inner core of the North Qinling Orogenic Belt(NQOB).Therefore,the Qinling Complex is the key to understanding the prePaleozoic evolution of the NQOB.The complex,which consists of metagraywackes and marbles,underwent regional amphibolite-facies metamorphism.In this study,we constrained the formation age of the Qinling Complex to the period between the late Mesoproterozoic and the early Neoproterozoic(ca.1062-962 Ma),rather than the Paleoproterozoic as previously thought.The LA-ICP-MS data show two major metamorphic ages(ca.499 and ca.420-400 Ma) for the Qinling Complex.The former age is consistent with the peak metamorphic age of the high- and ultra-high pressure(HP-UHP) rocks in the Qinling Complex,indicating that both the HP-UHP rocks and their country rocks experienced intensive regional metamorphism during the Ordovician.The latter age may constrain the time of partial melting in the NQOB between the late Silurian and early Devonian.The Qinling Complex is mostly affiliated with subduction-accretion processes along an active continental margin,and should contain detritus deposited in a forearc basin.The available data indicate that the NQOB was an independent micro-continent at least prior to the Neoproterozoic,and included a portion of the Grenville orogenic belt during the period of 1.2-0.8 Ga.The NQOB has experienced a unique geological history,which is obviously different from that of the North China Craton(NCC) and the Yangtze Craton during the Precambrian.The Neoproterozoic granitoids that intruded the Qinling Complex can be interpreted as the products of assembly of the supercontinent Rodinia.The NQOB was separated from Rodinia at ca.830-740 Ma.Subsequently,the NQOB moved closer to the northern margin of the NCC,and the initial accretion or collision with the NCC occurred from the late Cambrian to the early Ordovician. | Chunrong Diwu Yong Sun Yan Zhao BingXiang Liu Shaocong Lai | 2014 | Geoscience Frontiers2014，5，4： | 27 |
| 5 | Crustal growth at ~2.5 Ga in the North China Craton:evidence from whole-rock Nd and zircon Hf isotopes in the Huai'an gneiss terrane显示文摘Huai'an 片麻岩岩层主要由 TTG 片麻岩和 dioritic 片麻岩组成。在 magmatic 锆石核心标明日期的 situ U-Pb 的激光显示这些片麻岩的 protolith 在 ∼2.5 Ga 被形成。TTG 片麻岩有积极 ε 2.7 ~ 4.3 的 Nd (t) 价值,和大多数 magmatic 锆石有积极 ε 2.0 ~ 8.3 的 Hf (t) 价值。这些积极 ε Nd (t) 和 ε Hf (t) 价值两个都类似于在 2.5 Ga 的同时期的弄空的披风的那些。而且,为 magmatic 锆石的 2.44 ~ 2.73 Ga 的年轻 Hf 模型年龄接近预定锆石生长。整个岩石的 ε Nd (t) 价值由于在它的来源的古老的外壳的参与比在 TTG 片麻岩在 dioritic 片麻岩(0.8 ~ 1.7 ) 是更低的。然而,从 dioritic 片麻岩的许多 magmatic 锆石有类似的 ε Hf (t) 价值(2.0 ~ 7.9 ) 到同时代的弄空的披风的;他们 2.49 ~ 2.75 Ga 的 Hf 模型年龄接近锆石的 U-Pb 年龄。最高的 ε Hf (t) 价值接近弄空的披风,和相对高的 ε Hf (t) 价值对应于相对年轻的 Hf 模型年龄。这些 Nd 和 Hf 同位素特征建议 Huai'an 片麻岩岩层的片麻岩的这二种类型在 ca 从少年外壳发源。2.5 Ga。 | LIU Fu GUO JingHui LU XiaoPing DIWU ChunRong | 2009 | Chinese Science Bulletin2009，54，24： | 24 |
| 6 | ~4.1 Ga xenocrystal zircon from Ordovician volcanic rocks in western part of North Qinling Orogenic Belt显示文摘High-precision U-Pb dating by in situ LA-ICP-MS yields an age of 4079±5 Ma for a xenocrystal zircon from Ordovician volcanics of the Caotangou Group in western part of the North Qinling Orogenic Belt. As a result, the North Qinling Orogenic Belt becomes one of a few localities in the world that contain Hadean age records (4276±6 Ma and 4404±8 Ma detrital zircons from Jack Hill of the Yilgarn craton, 4016 Ma Acasta gneisses of the Wopmay Orogeny and Burang quartzite with detrital zircon of 4103 Ma in Tibet). It is also the first report of the Hadean age in Phanerozoic volcanics. The finding of the 4.1 Ga xenocrystal zircon provides not only the geochronological record of the oldest crustal materials in China, but also the condition for further search for rocks forming in the region during the early time of the Earth’s evolution. Thirty-six zircon U-Pb dates from the Ordovician volcanic rocks are subgrouped into seven generations that represent different tectono-magmatic events in the North Qinling Orogenic Belt. Among them, two periods of 0.9-1.5 Ga and 0.4-0.5 Ga are consistent with Mesoproterozoic and Early Paleozoic orogenies, respectively. | WANG HongLiang CHEN Liang SUN Yong LIU XiaoMing xu XueYi CHEN JuanLu ZHANG Hong DIWU ChunRong | 2007 | Chinese Science Bulletin2007，52，21： | 23 |
| 7 | Early Precambrian tectonothermal events of the North China Craton:Constraints from in situ detrital zircon U-Pb,Hf and O isotopic compositions in Tietonggou Formation显示文摘Clastic sediments and sedimentary rocks are widely used for understanding the formation and evolution of the continental crust.The Tietonggou Formation outcrops in the Xiaoqinling region at the southern margin of the North China Craton(NCC)and has unconformable contacts with the underlying Taihua Complex and overlying Paleoproterozoic Xiong’er Group.It mainly consists of quartzite and its protoliths are mature terrigenous clastic rocks.On the basis of the ages of the youngest detrital zircons from the quartzites and the ages of the Xiong’er Group,the depositional ages of the protoliths of the Tietonggou Formation were well constrained to 1.91–1.80 Ga.The U-Pb isotopic data of detrital zircons from the Formation show a major age peak at^2.1 Ga,which is consistent with 2.2–2.0 Ga magmatism in the Trans-North China Orogen of the NCC.Taking into account the texctural and compositional maturity of the Tietonggou Formation quartzite,the^2.1 Ga lithologic units in the Trans-North China Orogen are interpreted as the major source of the Tietonggou Formation.The majority of these^2.1 Ga detrital zircons mostly have highδ18O values(>6.5‰)and negativeεHf(t)values(–7.8–0.0),with corresponding Hf model ages significantly older than their crystallization ages,indicating that these zircons formed from the partial melting of ancient continental crust.The majority of the2.8–2.7 Ga and^2.5 Ga detrital zircons from the Tietonggou Formation had positiveεHf(t)values,and mantle-likeδ18O values,suggesting that the NCC has experienced two stages of significant crustal growth in the Neoarchaean at 2.7 and 2.5 Ga,respectively.The Hf isotopic data of detrital zircons from Paleoproterozoic metasedimentary rocks in the Trans-North China Orogen varied mainly toward the reduction of the radiogenic Hf isotope and gradually show a similar trend of the isotope trajectories of crustal evolution.This reveals that the NCC probably has not developed a long-lived subduction to complete the final assembly of the NCC.Alternatively,these maybe imply that the tectonic setting of the NCC substantially changed at^2.1 Ga,the reduction of the radiogenic Hf isotope could be attributed to the rollback of the subducting slab. | DIWU ChunRong SUN Yong GAO JianFeng FAN LongGang | 2013 | Chinese Science Bulletin2013，58，31： | 11 |
| 8 | Determination of trace and rare-earth elements in Chinese soil and clay reference materials by ICP-MS显示文摘Inductively coupled plasma mass spectrometry(ICP-MS) has become a powerful tool for providing reliable analytical results in many laboratories around the word. In this study, the mixture of HF and HNO3 acids in high-temperature and high-pressure closed-vessel digestion technique were used to decompose some Chinese reference materials, and thirty seven elements were determined by ICP-MS. Most of the results for Chinese soil reference materials were found to be in reasonable agreement with the reference values, except Cs, Ta, Li, Ge, Zn, Nd, Tb and Ta whose values need to be revised. Their precisions were typically lower than 5% RSD. However, the Precisions of Chinese clay reference materials, especially for GBW03102 and GBW03102a, were significantly different with reference values, probably reflecting the existence of a coarser-grained fraction(>70 μm) in samples, and the formation of fluorides in Al-rich samples during sample decomposition by using the mixture of HF and HNO3 acids. Moreover, thirty-seven trace elements covering the mass range from Li to U in four Chinese clay reference materials were firstly provided with good precision and accuracy in this study. | LIU Ye DIWU Chunrong ZHAO Yan LIU Xiaoming YUAN Honglin WANG Jianqi | 2014 | Chinese Journal Of Geochemistry2014，33，1： | 6 |
| 9 | Discovery of Neoproterozoic Rocks in the Dunhuang Block: Clues to Correlation with Rodinia显示文摘Objective Rodinia was a supercontinent that comprised nearly all the current existing continents/blocks on Earth to form a coherent large landmass during the Meso-Neoproterozoic. Thus, discovery of Meso-Neoproterozoic rocks in a certain Precambrian block can provide important clues for studying the assembly and break-up history of Rodinia. | WANG Tingyi DIWU Chunrong ZHAO Jian GAN Baoping | 2020 | Acta Geologica Sinica(English Edition)2020，94，4： | 1 |
| 10 | Magma mixing origin for the post-collisional adakitie monzogranite of the Triassic Yangba pluton, Northwest-ern margin of the South China block : Go- ehemistry,Sr-Nd isotopic, zircon U-Pb dating and Hf isotopic evi- dences 显示文摘 | Qin Jiangfeng Lai Shaocong Diwu Chunrong | 2010 | Contrib Mineral Petrol2010，159，3： | 1 |
| 11 | Episodic tec tonothermal events of the western north China Craton and north Qinling Orogenic Belt in central China: Constraints from detrital zircon U-Pb ages显示文摘 | Diwu Chunrong Sun Yong Zhang Hong | 2012 | Journal of Asian Earth Sci ences2012，47，： | 1 |
| 12 | Simultaneous determinations of U–Pb age, Hf isotopes and trace element compositions of zircon by excimer laser-ablation quadrupole and multiple-collector ICP-MS显示文摘 | Hong-Lin Yuan Shan Gao Meng-Ning Dai Chun-Lei Zong Detlef Günther Gisela Helene Fontaine Xiao-Ming Liu ChunRong Diwu | 2007 | Chemical Geology2007，，1： | 1 |
| 13 | Devonian continental arc magmatism in the southern Central Asian Orogenic Belt:Evidence from the Dunhuang Block,NW China显示文摘Reconstruction of periods and sources of continental arc magmatism provides critical insights for deciphering the thermal evolution and geodynamics of the continental lithosphere and unveiling subduction-related episodes of accretion and orogeny.The Dunhuang Block,located in the southern Central Asian Orogenic Belt,is built upon a Precambrian metamorphic crystalline basement that is intruded by numerous Paleozoic granitoids.In this paper,we present new zircon U-Pb ages,wholerock geochemistry and Sr-Nd-Pb-Hf isotopes from the Hanxiakouzi and Shuangta granodiorite plutons outcropped in the central and northern Dunhuang Block,respectively.The U-Pb zircon dating indicate that the Hanxiakouzi and Shuangta granodiorites were emplaced at ca.366–363 Ma,i.e.,in the late Devonian.Geochemically,the Hanxiakouzi granodiorites are medium-to high-K,I-type granites possessing high Sr and Sr/Y,i.e.,similar to adakites.The Hanxiakouzi granodiorites show negativeε_(Nd)(t)values(-8.2 to-6.6),significant positive eHf(t)values(+0.7 to+8.1),and evolved Pb isotope features suggesting their derivation by melting of subducted terrigenous sediments,interaction of melts with mantle peridotite,and assimilation of ancient crust during magma ascent.The Shuangta granodiorites belong to high-K calc-alkaline I-type granites with medium Sr and low Sr/Y.The Shuangta granodiorites yield negativeε_(Nd)(t)values(-2.9 to-3.1)and negative to positive zircon eHf(t)values(-1.8 to+3.6),suggesting their formation by partial melting of ancient mafic crust with addition of minor mantle-derived melt and subducted terrigenous sediments.In general,Hf-in-zircon isotopes characteristics of the late Paleozoic granitic rocks in the Dunhuang Block indicate that the southern Dunhuang area carries more ancient crust materials than the central and northern Dunhuang areas,indicating a lateral heterogeneity of the middle Paleozoic crust.Conclusively,the middle Paleozoic granitoids of the Dunhuang Block were emplaced at an active continental margin of the southern Paleo-Asian Ocean. | Baoping Gan Juxing Tang Inna Safonova Limao Qin Chunrong Diwu | 2023 | Geoscience Frontiers2023，14，6： | 0 |
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