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| 1 | Properties of oxide films grown on 25Cr20Ni alloy in air-H_2O and H_2-H_2O atmospheres显示文摘The oxidation kinetics, surface morphology and phase structure of oxide films grown on 25Cr20Ni alloy in air-H2O and H2-H2O atmospheres at 900 °C for 20 h were investigated. The anti-coking performance and resistance to carburization of the two oxide films were compared using 25Cr20Ni alloy tubes with an inner diameter of 10 mm and a length of 850 mm in a bench scale naphtha steam pyrolysis unit. The oxidation kinetics followed a parabolic law in an air-H2O atmosphere and a logarithm law in a H2-H2O atmosphere in the steady-state stage. The oxide film grown in the air-H2O atmosphere had cracks where the elements Fe and Ni were enriched and the un-cracked area was covered with octahedral-shaped MnCr2O4 spinels and Cr1.3Fe0.7O3 oxide clusters, while the oxide film grown in the H2-H2O atmosphere was intact and completely covered with dense standing blade MnCr2O4 spinels. In the pyrolysis tests, the anti-coking performance and resistance to carburization of the oxide film grown in the H2-H2O atmosphere were far better than that in the air-H2O atmosphere. The mass of coke formed in the oxide film grown in the H2-H2O atmosphere was less than 10% of that in the air-H2O atmosphere. The Cr1.3Fe0.7O3 oxide clusters converted into Cr23C6 carbides and the cracks were filled with carbon in the oxide film grown in the air-H2O atmosphere after repeated coking and decoking tests, while the dense standing blade MnCr2O4 spinels remained unchanged in the oxide film grown in the H2-H2O atmosphere. The ethylene, propylene and butadiene yields in the pyrolysis tests were almost the same for the two oxide films. | Wang Shenxiang Cui Lishan Wang Guoqing Zheng Yanjun Wang Hongxia Jia Jingsheng | 2014 | Petroleum Science2014，11，1： | 3 |
| 2 | New Cuprous Adsorbent Prepared by a Bioreduction Method for SOL Removal At Low Temperature显示文摘 | Lishan Jia Hao Song Qingbiao Li | 2008 | Industrial & Engineering Chemistry Research2008，47，22： | 1 |
| 3 | New cuprous adsorbent prepared by a bioreduction method for SO2 removal at low temperature显示文摘 | Jia Lishan Song Hao Li Qingbiao | 2008 | Ind Eng Chem Res2008，47，： | 1 |
| 4 | Seven new 3,4-dihydro-furanocoumarin derivatives from Angelica dahurica显示文摘Objective:To study the chemical constituents of the roots of Angelica dahurica,a well-known Chinese herbal medicine named Baizhi in Chinese.Methods:Compounds were separated by various chromatographies,and the structures of new compounds were elucidated based on the analysis of their spectroscopic and spectrometric data(1D,2D NMR,HRESI MS,IR,and UV).The absolute configurations of new compounds were determined by the calculated electronic circular dichroism and chemical derivatization.The inhibitory activities of all isolates against nitric oxide(NO)production were evaluated using lipopolysaccharide-activated RAW 264.7macrophage cells.Results:Seven new 3,4-dihydro-furanocoumarin derivatives(1a/1b,2a/2b,3a/3b,4)together with a known furanocoumarin(5)were isolated from the roots of A.dahurica.The new compounds included three pairs of enantiomers,(4S,2’’R)-angelicadin A(1a)/(4R,2’’S)-angelicadin A(1b),(4S,2’’S)-angelicadin A(2a)/(4R,2’’R)-angelicadin A(2b),and(4S,2’’S)-secoangelicadin A(3a)/(4R,2’’R)-secoangelicadin A(3b),together with(4R,2’’R)-secoangelicadin A methyl ester(4).The known xanthotoxol(5)inhibited the NO production with the half-maximal inhibitory concentration(IC50)value of(32.8±0.8)μmol/L,but all the new compounds showed no inhibitory activities at the concentration of100μmol/L.Conclusion:This is the first report of the discovery of 3,4-dihydro-furanocoumarins from A.dahurica.The results are not only meaningful for the understanding of the chemical constituents of A.dahurica,but also enrich the reservoir of natural products. | Yang Wang Fanyu Shi Zihan Lu Mingliang Zhang Zekun Zhang Fangfang Jia Beibei Zhang Lishan Ouyang Zhixiang Zhu Shepo Shi | 2023 | Chinese Herbal Medicines2023，15，3： | 1 |
| 5 | Stability analysisof efficient anti- collision protocol for RFID tag identifica-tion显示文摘 | Jia Xiaolin Feng Quanyuan Yu Lishan | 2012 | IEEE Transactions on Communications2012，60，8： | 1 |
| 6 | Visible-light-induced photocatalyst based on C-doped LaCoO3synthesizedby novel microorganism chelate methed显示文摘 | Jia Lishan Li Juanjuan Feng Weiping | 2009 | CatalysisCommunications2009，10，8： | 1 |
| 7 | Bio-oil from hydro-liquefaction of Dunaliella salina over Ni/REHY catalyst显示文摘 | YANY Chao JIA Lishan CHEN Changping | 2011 | Bioresource Technology2011，102，： | 1 |
| 8 | Large elastic strains and ductile necking of W nanowires embedded in TiNi matrix显示文摘The deformation behaviors of W nanowires embedded in a TiNi matrix were investigated by means of in-situ synchrotron high energy X-ray diffraction(HEXRD) and in-situ transmission electron microscopy(TEM) analysis during tensile deformation.The HEXRD measurement indicated that the W nanowires exhibited an average lattice strain of about 1.50 %,whereas the TEM examination revealed a local elastic strain of about 4.59 % in areas adjacent to the TiNi matrix where stress-induced martensitic transfo rmation occurred.This strain corresponds to a stress of ~15 GPa for the W nanowires.In addition,in areas adjacent to the TiNi matrix where plastic deformation and cracking were generated,the W nanowire showed significant ductile necking with ~80 % reduction in cross-section area.The ductile necking of W nanowire is attributed to the lack of protection from the stress-induced martensitic transformation of the TiNi matrix. | Daqiang Jiang Zhenghao Jia Hong Yang Yinong Liu Fangfeng Liu Xiaohua Jiang Yang Ren Lishan Cui | 2021 | Journal of Materials Science & Technology2021，，1： | 0 |
| 9 | Visbreaking of heavy petroleum oil catalyzed by SO_(4)^(2-)/ZrO_(2)solid super-acid doped with Ni^(2+) or Sn^(2+)显示文摘SO_(4)^(2-)/ZrO_(2) solid super-acid catalysts(SZ)doped with Ni^(2+)or Sn^(2+)(Ni^(2+)/SZ,Sn^(2+)/SZ)were prepared for catalytic visbreaking of heavy petroleum oil from Shengli oil field.The visbreaking reactions were carried out at 240uC and 3–4 MPa for 24 h using a heavy petroleum oil to catalyst mass ratio of 100:0.05.The effect of water content on viscosity of heavy petroleum oil was also investigated.Both catalysts can promote thermolysis of heavy petroleum oil and the viscosity was reduced from 0.319 Pa·s to 0.135 Pa?s for Ni^(2+)/SZ and 0.163 Pa·s for(Sn^(2+)/SZ)with visbreaking rates of 57.7% and 48.9%,respectively.After visbreaking,the saturated hydrocarbon content increased while aromatics,resin,asphaltene,sulfur and nitrogen content decreased.The presence of water was disadvantageous to visbreaking of heavy petroleum oil. | Ping JING Qingbiao LI Mei HAN Daohua SUN Lishan JIA Weiping FANG | 2008 | Frontiers of Chemical Science and Engineering2008，2，2： | 0 |
| 10 | Oxidation of Fe-Cr-Ni Alloys in a Low Oxygen Partial Pressure Atmosphere to Mitigate Coke Formation显示文摘Anti-coking oxide films were prepared on a 25Cr35Ni and 35Cr45Ni alloy surface under the low oxygen partialpressure atmosphere of a H2-H2O mixture. The composition and phase structure of the oxide films were analyzed by energydispersive spectroscopy (EDS), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The anti-cokingperformance of a mini tube made of a HP40 (25Cr35Ni) alloy was evaluated on a bench scale pyrolysis and coking test unit.The results showed that the surface Fe and Ni content decreased after the oxidation of the two alloys in a low oxygen partialpressure atmosphere. The oxide films were mainly composed of MnCr_(2)O_(4) and Cr_(2)O_(3). The average mass of coke in the minitube with oxide film decreased by 87% relative to that of a tube without an oxide film when the cracking temperature was 900℃. The ethylene, propylene, and butadiene yields in the pyrolysis tests were almost the same for the mini tubes withand without an oxide film. The oxide film on the alloy surface effectively inhibited catalytic filamentous coke formation.An industrial test showed that the run length of the cracking furnace with the in-situ coating technology was significantlyextended. | Wang Hongxia Wang Guoqing Zhang Lijun Wang Shenxiang Jia Jingsheng Cui Lishan | 2023 | China Petroleum Processing & Petrochemical Technology2023，25，3： | 0 |
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