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| 1 | Nb_(2)CT_(x) MXene: High capacity and ultra-long cycle capability for lithium-ion battery by regulation of functional groups显示文摘MXenes are well known for their potential application in supercapacitors due to their high-rate intercalation pseudocapacitance and long cyclability.However,the reported low capacity of pristine MXenes hinders their practical application in lithium-ion batteries.In this work,a robust strategy is developed to control the functional groups of Nb_2 CT_x MXene.The capacity of pristine Nb_2 CT_x MXene can be significantly increased by Li~+ intercalation and surface modification.The specific capacity of the treated Nb_2 CT_x is up to 448 mAh g^(-1) at 0.05 A g^(-1),and at a large current density of 2 A g^(-1) remains a high reversible capacity retention rate of 75% after an ultra-long cycle of 2000 cycles.These values exceed most of the reported pristine MXenes(including the most studied Ti_3 C_2 T_x) and carbon-based materials.It demonstrates that this strategy has great help to improve the electrochemical performance of pristine MXene,and the results enhance the promise of MXenes in the application of lithium-ion batteries. | Jiabao Zhao Jing Wen Junpeng Xiao Xinzhi Ma Jiahui Gao Lina Bai Hong Gao Xitian Zhang Zhiguo Zhang | 2021 | Journal of Energy Chemistry2021，30，2： | 2 |
| 2 | Extraction Process and Content Determination of Caffeic Acid in Laggera alata from Different Production Areas of Guangxi显示文摘[Objectives] To establish a method for determining the content of Laggera alata( D. Don) Sch. Bip. Ex Oliv. using caffeic acid the target component,and to compare the content of caffeic acid in the medicinal materials of L. alata in different production areas of Guangxi.[Methods]The content was determined by Inertsil~ODS-3 chromatographic column C_(18)( 4. 60 mm × 250 mm,5 μm,mobile phase: acetonitrile-0. 1% phosphoric acid( 22∶ 78),detection wavelength: 320 nm,flow rate: 1. 0 m L/min,column temperature: 30℃,and injection volume: 10 μL. [Results] The caffeic acid showed a good linear relationship in the range of injection volume of 0. 025 92-0. 259 2 μg( R =0. 999 5). The average recovery rate was 98. 33%( RSD = 1. 85%). L. alata in different production areas of Guangxi contained the caffeic acid,and there was a great difference in the caffeic acid. L. alata in Baise had the highest content of caffeic acid,while that in Guilin had the lowest content of caffeic acid. [Conclusions]This method can accurately determine the content of caffeic acid and is expected provide a scientific basis for the development and utilization of herbal medicine L. alata. | Jiangcun WEI Yong CHEN Zujie QIN Jiabao MA Shengbin CHEN Zuliang QUE Jinzhou LI Zijun CHEN | 2018 | Medicinal Plant2018，9，4： | 1 |
| 3 | Disturbed gut virome with potent interferonogenic property in systemic lupus erythematosus显示文摘Accumulating evidence suggests an essential role of disturbed gut microbiota in the etiopathogenesis of systemic lupus erythematosus(SLE),but it remains unclear as to gut virome.In this study,fecal virus-like particles(VLPs)isolated from 76 non-treated SLE patients and 75 healthy controls were subjected to gut virome profiling.The proportion of bacteriophages was significantly elevated in the SLE gut,and the altered viral taxa were correlated with clinical parameters.Gut virome and bacteriome were closely associated with each other in SLE patients.The combination of gut viral and bacterial markers displayed better performance in distinguishing SLE patients from healthy controls.Further,VLPs from non-treated SLE patients promoted interferon-a production in an epithelial cell line and human immune cells.Intriguingly,the interferon-stimulatory capacity diminished in VLPs from post-treated SLE patients.Our findings may shed novel insights into SLE pathogenesis.Further in-depth understanding of gut virome might help develop future biomarkers and therapeutics for SLE patients. | Beidi Chen Jiabao Cao Wei Liu Yuqing Zhang Yudong Liu Min Wang Fei Xiao Jie Ma Jun Wang Xuan Zhang | 2023 | Science Bulletin2023，，3： | 1 |
| 4 | High sulfur loading and shuttle inhibition of advanced sulfur cathode enabled by graphene network skin and N,P,F-doped mesoporous carbon interfaces for ultra-stable lithium sulfur battery显示文摘Achieving high loading of active sulfur yet rational regulating the shuttle effect of lithium polysulfide(LiPS)is of great significance in pursuit of high-performance lithium-sulfur(Li-S)battery.Herein,we develop a free-standing graphene nitrogen(N),phosphorus(P)and fluorine(F)co-doped mesoporous carbon-sulfur(G-NPFMC-S)film,which was used as a binder-free cathode in Li-S battery.The developed mesoporous carbon(MC)achieved a high specific surface area of 921 m^(2)·g^(-1)with a uniform pore size distribution of 15 nm.The inserted graphene network inside G-NPFMC-S cathode can effectively improve its electrical conductivity and simultaneously restrict the shuttle of LiPS.A high sulfur loading of 86%was achieved due to the excellent porous structures of graphene-NPFMC(G-NPFMC)composite.When implemented as a freestanding cathode in Li-S battery,this G-NPFMC-S achieved a high specific capacity(1,356 mAh·g^(-1)),favorable rate capability,and long-term cycling stability up to 500 cycles with a minimum capacity fading rate of 0.025%per cycle,outperforming the corresponding performances of NPFMC-sulfur(NPFMC-S)and MC-sulfur(MC-S).These promising results can be ascribed to the featured structures that formed inside G-NPFMC-S film,as that highly porous NPFMC can provide sufficient storage space for the loading of sulfur,while,the N,P,F-doped carbonic interface and the inserted graphene network help hinder the shuttle of LiPS via chemical adsorption and physical barrier effect.This proposed unique structure can provide a bright prospect in that high mass loading of active sulfur and restriction the shuttle of LiPS can be simultaneously achieved for Li-S battery. | Haotian Liu Fan Liu Zehua Qu Jieling Chen Hui Liu Yiqing Tan Jiabao Guo Yan Yan Shuang Zhao Xinsheng Zhao Xinming Nie Xin Ma Zengxia Pei Mingkai Liu | 2023 | Nano Research Energy2023，2，1： | 1 |
| 5 | Quality Standard of Fuyang Wenshen Granules显示文摘[Objectives]To establish the quality standard of Fuyang Wenshen Granules and carry out the routine examination of granule type.[Methods]The particle size,water content,solubility,loading difference and microbial limit of Fuyang Wenshen Granules were examined,and TLC was used for qualitative identification of Astmgali Radix and Notoginseng Radix Et Rhizoma.[Results]The particle size,water content,solubility,loading difference,and microbial limit of Fuyang Wenshen Granules complied with the relevant provisions of the Pharmacopoeia of the People's Republic of China(2020).The TLC spots of Astmgali Radix and Notoginseng Radix Et Rhizoma were clearly colored,and negative had no interference.[Conclusions]The method was simple,accurate,reliable,specific and reproducible,and can effectively control the quality of Fuyang Wenshen Granules. | Wei CHEN Jing FU Xiaoxia LI Jinhua LIU Jiabao MA Yueqiang HU | 2023 | Medicinal Plant2023，14，2： | 0 |
| 6 | Control Effect of UAV Low Volume Spray Technology on Thrips and Tomato Spotted Wilt Virus in Tobacco Field显示文摘[Objectives]The paper was to explore the influence of unmanned aerial vehicle(UAV)low volume spray technology on the control effect of viruliferous thrips and tomato spotted wilt virus(TSWV)under different pesticide concentrations,and to explore the effective control nodes and methods of thrips and TSWV.[Methods]According to the occurrence characteristics of thrips and TSWV,the field control effects of 4 pesticides on thrips and TSWV were tested by UAV with the thrips number and disease index as indicators,following the principle of regional and periodic control trials.[Results]In the groups of UAV and artificial prevention and control,4 agents were used alternatively,including 1%emamectin benzoate ME,1.7%abamectin imidacloprid ME,5%emamectin benzoate WDG,and 30%pyriproxyfen dinotefuran SL.There was no significant difference in the control effect of thrips and TSWV among treatment 1(recommended dosage of UAV agent),treatment 2(reduction of recommended dosage of UAV agent by 25%)and treatment 4(recommended dosage of artificial control agent),and the control effects on thrips were more than 83.16%in the 3 treatments.The disease index of TSWV in the 3 treatments decreased from 8.64±1.37 in the blank control group to less than 3,which reached the prevention and control threshold.But treatment 3(reduction of recommended dosage of UAV agent by 50%)did not reach the prevention and control threshold.The disease index of TSWV in the blank control area increased with the increase of the number of live nymphs of thrips,and there was a significant positive correlation,with good fitness.[Conclusions]UAV has a significant impact on the control effect of thrips and TSWV under different pesticide concentrations.In the actual flight control application,it is recommended that the amount of the pesticides is about 3/4 and not less than 1/2 of that of the artificial application.The control area should be extended to 100 m of the ridge of the tobacco field,and UAV is used periodically to control thrips and TSWV for 5 times from pre-transplanting stage to pre-squaring stage of flue-cured tobacco.The control effect is significantly different from the traditional artificial application. | Zefan LIU Dean XIE Jiabao HAN Yanfen XIE Li MA Siyuan GAO Ruiqi PENG Yuting ZHAO Xiangze FU Wengang CHENG Yonghong FENG Yan ZHANG Huaping ZHANG Ying HUANG Leijie DAI Lanfeng WANG | 2023 | Plant Diseases and Pests2023，14，4： | 0 |
| 7 | Skin Toxicity of Wufang Babu Ointment to Zebrafish显示文摘[Objectives]Using wild-type AB strain of zebrafish as experimental animal,this study investigated the damaging effect of Wufang Babu Ointment on skin cells,in order to evaluate the skin toxicity of Wufang Babu Ointment.[Methods]Wild-type AB strain of zebrafish with an age of 2 d were taken and fed in different concentrations of Wufang Babu Ointment solution for 24 h.The number of deaths in each group of zebrafish was recorded,and the mortality rate was calculated.Using Origin 8.0 software,the maximum non lethal concentration(MNLC)was simulated.Zebrafish raised in different concentrations of Wufang Babu Ointment solution for 24 h were placed under an anatomical microscope for taking photos,to analyze and calculate the incidence of skin damage in zebrafish.Based on the statistical analysis results of this indicator,the skin toxicity of Wufang Babu Ointment was evaluated.[Results]The MNLC of Wufang Babu Ointment on zebrafish was 671μg/mL;Wufang Babu Ointment can induce skin damage at the concentrations of 224μg/mL(1/3 MNLC)and 671μg/mL(MNLC).[Conclusions]Wufang Babu Ointment had certain skin toxicity to zebrafish. | Xiaoxia LI Jiabao MA Jing FU Jinhua LIU Xiongbin GUI | 2024 | Medicinal Plant2024，15，2： | 0 |
| 8 | Typical HPLC Chromatogram of Petroleum Ether in Abutilon indicum(L.) Sweet from Different Habitats显示文摘[Objectives] To study the typical HPLC chromatogram of petroleum ether in Abutilon indicum (L.) Sweet from different habitats, in order to provide experimental basis for the quality control of A. indicum and the spectrum-efficacy relationship of petroleum ether.[Methods] The HPLC chromatogram of petroleum ether was obtained using Agilent SB-C 18 (4.6 mm×250 mm, 5 μm) and acetine-0.1% phosphoric acid solution for gradient elution at temperature of 30 ℃, flow rate of 1.0 mL/min and detection wavelength of 205 nm.[Results] The typical HPLC chromatogram of petroleum ether in A. indicum was preliminarily established, with 12 characteristic peaks. It was verified by A. indicum from different habitats, characterized by reproducibility and stability.[Conclusions] Typical HPLC chromatogram provides a stable new method for the quality control of petroleum ether in A. indicum . This study provides experimental basis for further study on the medicinal parts of A. indicum . | Yong CHEN Jiabao MA Jiangcun WEI Qian HAN | 2019 | Medicinal Plant2019，10，4： | 0 |
| 9 | Study on damage-stress loss coupling model of rock and prestressed anchor cable in dry-wet environment显示文摘The loss of anchoring force is one of the problems to be solved urgently.The anchorage loss is a key factor causing the failure of anchoring engineering,so it is crucial to study the time-dependent variation of anchoring force.Alternating dry and wet(D-W)conditions have a significant effect on deformation of rock.The anchoring system is composed of anchoring components and rock mass,and thus rock deformation has a significant impact on the loss of anchoring force.Quantifying rock deformation under the effects of D-W cycles is a prerequisite to understanding the factors that influence loss of anchoring force in anchor bolts.In this study,we designed an anchoring device that enabled real-time monitoring of the variation in strain during D-W periods and rock testing.Nuclear magnetic resonance(NMR)measurements showed that under D-W conditions,the increment in porosity was smaller for prestressed rock than unstressed rock.The trends of prestress loss and strain variation are consistent,which can be divided into three characteristic intervals:rapid attenuation stage,slow attenuation stage and relatively stable stage.At the same stress level,the rate of stress loss and strain for the soaking specimen was the highest,while that of the dried specimen was the lowest.In the same D-W cycling conditions,the greater the prestress,the smaller the strain loss rate of the rock,especially under soaking conditions.The characteristics of pore structure and physical mechanical parameters indicated that prestress could effectively suppress damage caused by erosion related to D-W cycles.The study reveals the fluctuation behavior of rock strain and prestress loss under D-W conditions,providing a reference for effectively controlling anchoring loss and ideas for inventing new anchoring components. | Yu Zhao Huasu Wang Jing Bi Zhijun Wu Chaolin Wang Jiabao Ma | 2023 | International Journal of Mining Science and Technology2023，33，12： | 0 |
| 10 | Preliminary Study and Quality Analysis of Laggera alata显示文摘[Objectives]To establish a method for quality analysis of Laggera alata.[Methods]The water content,total ash and alcohol-soluble extract of Laggera alata were determined according to the method of 2015 edition of Chinese Pharmacopoeia.[Results]Ten batches of Laggera alata from different producing areas and different collection time in Guangxi had the same plant morphology and medicinal properties.The experimental results were as follows:the water content was 5.19%-10.86%;the total ash content was 5.91%-10.74%;the acid-insoluble ash content was 0.44%-0.92%;the extract content was 14.64%-19.95%.[Conclusions]The experimental results can provide scientific basis for the development and utilization of Laggera alata and the establishment of its quality standard. | Jiangcun WEI Jiabao MA Jian CUI Zhenying FU Xianyi SHI Yan MA Lifu WEI Zhengteng YANG | 2020 | Medicinal Plant2020，11，3： | 0 |
| 11 | Thin-layer Identification,Extraction Process and Content Determination of Chlorogenic Acid in Laggera alata(D.Don)Sch.Bip.ex Oliv.显示文摘[Objectives]This paper aims to establish thin-layer identification and content determination method for Laggera alata(D.Don)Sch.Bip.ex Oliv.with chlorogenic acid as the index component and compare the content of chlorogenic acid in L.alata from different places in Guangxi.[Methods]Silica gel GF254 thin-layer plate was used for identification under an ultraviolet lamp(365 nm),with butyl acetate-formic acid-water(V∶V∶V=7∶2.5∶2.5)as a developing agent.The content of chlorogenic acid was determined under the following chromatographic conditions:column,Inertsil ODS-3 C18 column(4.60 mm×250 mm,5μm);mobile phase,methanol-0.1%phosphoric acid(28∶72);detection wavelength,329 nm;flow rate,1.0 mL/min;column temperature,25℃;and injection volume,10μL.[Results]Chlorogenic acid can be detected by thin layer chromatography with clear spot and good specificity.Chlorogenic acid showed a good linear relationship in the injection amount range of 0.099-0.99μg(R^(2)=0.9999).The content of chlorogenic acid in L.alata varied greatly among the 10 different producing areas in Guangxi.L.alata produced in Dee Township,Longlin,Baise,Guangxi showed the highest chlorogenic acid content,and that produced in Shangsi County and Pingle County showed the lowest chlorogenic acid content.[Conclusions]This method can effectively identify L.alata and accurately determine the content of chlorogenic acid,thereby providing a scientific basis for the development and utilization of L.alata resources. | Qiaofeng QIN Xue JIANG Jiangcun WEI Jiabao MA Jingrong LU Lifu WEI Xiumei MA Xuanyang ZENG | 2020 | Medicinal Plant2020，11，6： | 0 |
| 12 | Study on the Quality Standard of Dujieqing Pill显示文摘[Objectives]To establish the quality control method of Dujieqing pills.[Methods]Tangerine peel and Panax notoginseng in Dujieqing pills were qualitatively identified by thin layer chromatography(TLC).The content of hesperidin and ginsenoside Rb1 was determined by HPLC.The acetonitrile-aqueous solution was used as mobile phase for gradient elution,the detection wavelength was 203 nm,the flow rate was 1.0 mL/min,the column temperature was 25℃,and the injection volume was 10μL.[Results]Under TLC,tangerine peel and P.notoginseng had clear chromatographic spots,good separation effect,and strong specificity and negative samples showed no interference;there was a good linear relationship between hesperidin and ginsenoside Rb1 in the range of 0.838-8.38μg(R2=0.9994)and 0.44-4.4μg(R2=0.9994),respectively;the average recovery(n=9)was 98.90%(RSD=2.31%)and 98.31%(RSD=2.56%),respectively.[Conclusions]The established quality control method is simple,reproducible,accurate and reliable,and can be used for the quality control of Dujieqing pills. | Fengxian ZHAO Jiabao MA Jiangcun WEI Xianxian LIU Wenli LI Yong CHEN Zhengteng YANG | 2021 | Medicinal Plant2021，12，4： | 0 |
| 13 | Cache-Enabled in Cooperative Cognitive Radio Networks for Transmission Performance显示文摘The proliferation of mobile devices that support the acceleration of data services(especially smartphones)has resulted in a dramatic increase in mobile traffic. Mobile data also increased exponentially, already exceeding the throughput of the backhaul. To improve spectrum utilization and increase mobile network traffic, in combination with content caching, we study the cooperation between primary and secondary networks via content caching. We consider that the secondary base station assists the primary user by pre-caching some popular primary contents.Thus, the secondary base station can obtain more licensed bandwidth to serve its own user. We mainly focus on the time delay from the backhaul link to the secondary base station. First, in terms of the content caching and the transmission strategies, we provide a cooperation scheme to maximize the secondary user’s effective data transmission rates under the constraint of the primary users target rate. Then, we investigate the impact of the caching allocation and prove that the formulated problem is a concave problem with regard to the caching capacity allocation for any given power allocation. Furthermore, we obtain the joint caching and power allocation by an effective bisection search algorithm. Finally, our results show that the content caching cooperation scheme can achieve significant performance gain for the primary and secondary systems over the traditional two-hop relay cooperation without caching. | Jiachen Yang Chaofan Ma Jiabao Man Huifang Xu Gan Zheng Houbing Song | 2020 | Tsinghua Science and Technology2020，25，1： | 0 |
| 14 | Preliminary Study on Quality Analysis of Guangxi Zhuang Medicine Lysimachia foenum-graecum Hance显示文摘[Objectives]To establish a quality analysis method for Guangxi Zhuang medicine Lysimachia foenum-graecum Hance.[Methods]The moisture,total ash and alcohol-soluble extracts of L.foenum-graecum medicinal materials were determined in accordance with the inspection method of the Chinese Pharmacopoeia(2015).[Results]The 10 batches of L.foenum-graecum medicinal materials from different origins and different collection times in Guangxi all had the same plant morphology and medicinal properties.The moisture content was 5.69%-10.51%,the total ash content was 5.50%-8.61%,the acid-insoluble ash content was 0.42%-0.78%,and the extract was 15.28%-20.75%.[Conclusions]This study is expected to provide a scientific basis for the development and utilization of L.foenum-graecum medicinal materials and the establishment of its quality standards. | Jiabao MA Xiumei MA Zhengteng YANG Wen ZHONG Chenglong WANG Jiangcun WEI | 2021 | Medicinal Plant2021，12，5： | 0 |
| 15 | Quality Standard Research of Shenqi Qiangjing Granules显示文摘[Objectives]The paper was to establish the quality standard of Shenqi Qiangjing granules and to conduct routine inspection of granular dosage forms.[Methods]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were detected.Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis were qualitatively identified by thin layer chromatography(TLC).[Results]The particle size,moisture,loss on drying,dissolubility,content uniformity and microbial limit of Shenqi Qiangjing granules were all in line with the relevant regulations of Pharmacopoeia of the People's Republic of China(2020 edition).Radix Astragali,Herba Epimedii,Radix Dipsaci and Fructus Schisandrae Chinensis had clear fluorescent spots in TLC assay,and no such spots were found in negative control.[Conclusions]The method has the advantages of simple operation,accurate and reliable results,strong specificity and good repeatability,and can effectively control the quality of Shenqi Qiangjing granules. | Jinhua LIU Min HUANG Jiabao MA Bin BIN Xiaoxia LI Jing FU Aicun TANG | 2023 | Medicinal Plant2023，14，1： | 0 |
| 16 | Determination of the Content of Five Active Components in Toad Skin显示文摘[Objectives] To establish a method for the determination of active components in toad skin. [Methods] HPLC method was used to determine the content of five active components (bufotalin, cinobufotalin, bufalin, cinobufagin and resibufogenin) in toad skin. [Results] Chromatographic conditions are as follows: Agilent ZORBAX SB-C 18 chromatographic column was used;acetonitrile (A)-0.3% glacial acetic acid (B) gradient elution (0-15 min, 28%A-54%A;15-35 min, 54%A-54%A) was conducted;the flow rate was 0.6 mL/min;the detection wavelength was 296 nm;the column temperature was 30 ℃;the sample size was 10 μL. Under the above conditions, the determination method of the five components can be established at one time. [Conclusions] The method was stable and reliable, and can provide experimental basis for the development and utilization of active ingredients in toad skin. | Xue JIANG Wenli LI Yong CHEN Jiabao MA | 2023 | Medicinal Plant2023，14，4： | 0 |
| 17 | Long-term Toxicity of Maxing Erchen Zhike Granules显示文摘[Objectives]To study the long-term toxicity of Maxing Erchen Zhike granules to rats after intragastric administration,so as to provide reference for its preclinical safety evaluation.[Methods]Total 80 rats were randomly and evenly divided into high-dose group(1.2 mL/100 g,120 g/kg),middle-dose group(96.0 g/kg),low-dose group(72.0 g/kg)and blank control group.The rats in the treatment groups were administered with corresponding doses of Maxing Erchen Zhike granules,and those in the blank control group were given with equal-amount normal saline.The administration lasted for 30 consecutive days.During the experiment,the rats'feed intake,activity,feces and other conditions and toxicity reactions were observed every day.After 24 h of the last administration,12 rats(half male and half female)were randomly selected from each group.Each of the rats was anesthetized with 10%chloral hydrate solution(0.3 mL/100 g)through intraperitoneal injection and subjected to abdominal aorta blood collection(two tubes)for hematological examination and blood biochemical examination(serum).Then,the main organs of the rats were weighed,and pathological examinations were performed.After that,the main organs were weighed and pathological examination was performed.The remaining rats in each group were discontinued and observed for 14 d.On the 15th d,they were subjected to the same treatment,and the body weight,organ coefficients,hematological indices,blood biochemical indices and pathological indices were examined.[Results]After 30 d of administration,there was no abnormality in the appearance and behavior of the animals.There was no significant difference in the daily consumption of feed among the groups,and there was no special case of weight gain.Among the blood biochemical indices,the ALB and ALT levels of each administration group were significantly different from those of the blank control group(P<0.05).The results of histopathological examination show that there was one case of interstitial pneumonia in each of the high-dose group,middle-dose group and blank control group.After 14 d that the administration was stopped,one case of focal myocarditis appeared in the high-dose group,and one case of interstitial pneumonia appeared in the middle-dose group.[Conclusions]Maxing Erchen Zhike granules are safe to be administered to rats at 100 times the clinical dose.and there should be no safety hazards clinically when used at conventional doses. | Jiabao MA Zhenyuan WEI Shuang WU Jiahuan WEI Shengbin CHEN Jinhua LIU Zhengteng YANG | 2020 | Medicinal Plant2020，11，5： | 0 |
| 18 | Effect of Different Processing Methods on Content ofβ-Asarone in the Zhuang Medicine Rhizoma Acori Tatarinowii显示文摘[Objectives]This paper aims to establish a method to simultaneously determine the content ofβ-asarone in Rhizoma Acori Tatarinowii dried by three different methods.[Methods]Reversed-phase high-performance liquid chromatography was used,and the chromatographic conditions were as follows:column,Thermo SCIENTIFIC Hypersil GOLD Dim.(mm);mobile phase,methanol-0.1%phosphoric acid(63∶37);column temperature,30℃;flow rate,1mL/min;detection wavelength,257 nm;sample size,10μL.[Results]The linear range of the injection volume ofβ-asarone was 49.28-246.40μg/mL(R=0.9993);the limit of quantification was 0.85 ng and the detection limit was 0.34 ng;the RSD values of precision,stability and reproducibility tests were all less than 3%;and the sample recovery rate was 98.53%-98.97%(RSD<3.00).The results show that the content ofβ-asarone was highest in shade-dried Rhizoma Acori Tatarinowii.The order ofβ-asarone content was as follows:Rhizoma Acori Tatarinowii dried in shade>Rhizoma Acori Tatarinowii dried at 55℃>Rhizoma Acori Tatarinowii dried at 60℃.[Conclusions]This method is sensitive,reliable,and reproducible.It can be used to simultaneously determine the content ofβ-asarone in Rhizoma Acori Tatarinowii dried by three different methods. | Peng YANG Jiangcun WEI Wen ZHONG Xiumei MA Xuelan LUO Peitao XIE Jiabao MA Qian HAN | 2020 | Medicinal Plant2020，11，5： | 0 |
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