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| 1 | Altered trends in carbon uptake in China’s terrestrial ecosystems under the enhanced summer monsoon and warming hiatus显示文摘The carbon budgets in terrestrial ecosystems in China are strongly coupled with climate changes.Over the past decade,China has experienced dramatic climate changes characterized by enhanced summer monsoon and decelerated warming.However,the changes in the trends of terrestrial net ecosystem production(NEP)in China under climate changes are not well documented.Here,we used three ecosystem models to simulate the spatiotemporal variations in China's NEP during 1982–2010 and quantify the contribution of the strengthened summer monsoon and warming hiatus to the NEP variations in four distinct climatic regions of the country.Our results revealed a decadal-scale shift in NEP from a downtrend of–5.95 Tg C/yr^2(reduced sink)during 1982–2000 to an uptrend of 14.22 Tg C/yr^2(enhanced sink)during 2000–10.This shift was essentially induced by the strengthened summer monsoon,which stimulated carbon uptake,and the warming hiatus,which lessened the decrease in the NEP trend.Compared to the contribution of 56.3%by the climate effect,atmospheric CO2 concentration and nitrogen deposition had relatively small contributions(8.6 and 11.3%,respectively)to the shift.In conclusion,within the context of the global-warming hiatus,the strengthening of the summer monsoon is a critical climate factor that enhances carbon uptake in China due to the asymmetric response of photosynthesis and respiration.Our study not only revealed the shift in ecosystem carbon sequestration in China in recent decades,but also provides some insight for understanding ecosystem carbon dynamics in other monsoonal areas. | Honglin He Shaoqiang Wang Li Zhang Junbang Wang Xiaoli Ren Lei Zhou Shilong Piao Hao Yan Weimin Ju Fengxue Gu Shiyong Yu Yuanhe Yang Miaomiao Wang Zhongen Niu Rcmg Ge Huimin Yan Mei Huang Guoyi Zhou Yongfei Bai Zongqiang Xie Zhiyao Tang Bingfang Wu Leiming Zhang Nianpeng He Qiufeng Wang Guirui Yu | 2019 | National Science Review2019，6，3： | 24 |
| 2 | A BRIEF REVIEW AND PROSPECT OF EXPERIMENTAL SOLID MECHANICS IN CHINA显示文摘In this review,a critical look at the research progress of experimental solid mechanics in China for the past years is presented.Issues are discussed of the discovery and development of new fundamental methods and techniques versus performance benchmarking for many of their applications.Included herein are photoelasticity and various forms of modern photomechanics,acoustical techniques,image processing and videometrics,radial and spectrum techniques,and experimental mechanics on micro/nano scale.It is also noticed that both the ever developed instrumentation and specialized synthetical techniques have played important roles in advancing experimental mechanics in scientific researches and industrial applications.Finally,an attempt is made to look into the future of experimental solid mechanics with personal opinions offered on what the future trends will be for the researches in the field. | Xide Li Huimin Xie Yilan Kang Xiaoping Wu | 2010 | Acta Mechanica Solida Sinica2010，23，6： | 17 |
| 3 | Zircon U-Pb dating of basement gneisses in the super-large Bayan Obo REE-Fe-Nb deposit, Inner Mongolia显示文摘Zircon U-Pb ages have been determined for basement gneisses in the Bayan Obo REE-Fe-Nb deposit. On the U-Pb concordia diagram data of three samples yield up-per intercept ages of 1948-1917 Ma. Thus, these basement gneisses are of Paleoproterozoic. Rock association of these basement gneisses includes tonalite, syenite and paragneiss, not belonging to a sedimentary package. It is more appro-priate to consider this association as a basement complex rather than a stratigraphic 'Group'. | WANG Kaiyi FAN Hongrui XIE Yihan LI Huimin | 2002 | Chinese Science Bulletin2002，47，3： | 16 |
| 4 | Preparation of Zn-doped TiO_2 nanotubes electrode and its application in pentachlorophenol photoelectrocatalytic degradation显示文摘Zn-doped titanium oxide (TiO2) nanotubes electrode was prepared on a titanium plate by direct anodic oxidation and immersing method in sequence. Field emission scanning electron microscopy (FESEM) showed that the Zn-doped TiO2 nanotubes were well aligned and organized into high density uniform arrays with diameter ranging from 50 to 90 nm. The length and the thickness were about 200 and 15 nm respectively. TiO2 anatase phase was identified by X-ray diffraction (XRD). X-ray photoelectronspec-troscopy (XPS) indicated that Zn ions were mainly located on the surface of TiO2 nanotubes in form of ZnO clusters. Compared with TiO2 nanotubes electrode,about 20 nm red shift in the spectrum of UV-vis absorption was observed. The degradation of pentachlorophenol (PCP) in aqueous solution under the same condition (initial concentration of PCP: 20 mg/L; concentration of Na2SO4: 0.01 mol/L and pH: 7.03) was carried out using Zn-doped TiO2 nanotubes electrode and TiO2 nanotubes electrode. The degradation rates of PCP using Zn-doped TiO2 nanotubes electrode were found to be twice and 5.8 times as high as that using TiO2 nanotubes electrode by UV radiation (400 μw/cm2) and visible light radiation (4500 μw/cm2),respectively. 73.5% of PCP was removed using Zn-doped TiO2 nanotubes electrode against 48.5% removed using TiO2 nanotubes electrode in 120 min under UV radiation. While under visible light radiation,the degradation efficiency of PCP was 18.4% using Zn-doped TiO2 nano-tubes electrode against 3.2% using TiO2 nanotubes electrode in 120 min. The optimum concentration of Zn doping was found to be 0.909%. The PCP degradation efficiencies of the 10 repeated experiments by Zn-doped TiO2 nanotubes electrode were rather stable with the deviation within 3.0%. | ZHAO HuiMin CHEN Yue QUAN Xie RUAN XiuLi | 2007 | Chinese Science Bulletin2007，52，11： | 14 |
| 5 | Impact of dissolved organic matter on the photolysis of the ionizable antibiotic norfloxacin显示文摘Norfloxacin(NOR), an ionizable antibiotic frequently used in the aquaculture industry, has aroused public concern due to its persistence, bacterial resistance, and environmental ubiquity.Therefore, we investigated the photolysis of different species of NOR and the impact of a ubiquitous component of natural water — dissolved organic matter(DOM), which has a special photochemical activity and normally acts as a sensitizer or inhibiter in the photolysis of diverse organics; furthermore, scavenging experiments combined with electron paramagnetic resonance(EPR) were performed to evaluate the transformation of NOR in water. The results demonstated that NOR underwent direct photolysis and self-sensitized photolysis via hydroxyl radical(U OH) and singlet oxygen(1O2) based on the scavenging experiments. In addition, DOM was found to influence the photolysis of different NOR species, and its impact was related to the concentration of DOM and type of NOR species. Photolysis of cationic NOR was photosensitized by DOM at low concentration, while zwitterionic and anionic NOR were photoinhibited by DOM, where quenching of U OH predominated according to EPR experiments, accompanied by possible participation of excited triplet-state NOR and1O2. Photo-intermediate identification of different NOR species in solutions with/without DOM indicated that NOR underwent different photodegradation pathways including dechlorination, cleavage of the piperazine side chain and photooxidation, and DOM had little impact on the distribution but influenced the concentration evolution of photolysis intermediates. The results implied that for accurate ecological risk assessment of emerging ionizable pollutants, the impact of DOM on the environmental photochemical behavior of all dissociated species should not be ignored. | Chen Liang Huimin Zhao Minjie Deng Xie Quan Shuo Chen Hua Wang | 2015 | Journal of Environmental Sciences2015，27，1： | 11 |
| 6 | Simulation of residual stresses and their effects on thermal barrier coating systems using finite element method显示文摘Thermal barrier coating(TBC)systems are widely used in industrial gas-turbine engines.However,premature failures have impaired the use of TBCs and cut down their lifetime,which requires a better understanding of their failure mechanisms.In the present study,experimental studies of isothermal cycling are firstly carried out with the observation and estimation of microstructures.According to the experimental results,a finite element model is established for the analysis of stress perpendicular to the TBC/BC interface.Detailed residual stress distributions in TBC are obtained to reflect the influence of mechanical properties,oxidation,and interfacial roughness.The calculated results show that the maximum tensile stress concentration appears at the peak of TBC and continues to increase with thermal cycles.Because of the microstructural characteristics of plasma-sprayed TBCs,cracks initialize in tensile stress concentration(TSC)regions at the peaks of TBC and propagate along the TBC/BC interface resulting in the spallation of TBC.Also,the inclusion of creep is crucial to failure prediction and is more important than the inclusion of sintering in the simulation. | ZHU JianGuo CHEN Wei XIE HuiMin | 2015 | Science China(Physics,Mechanics & Astronomy)2015，58，3： | 11 |
| 7 | RECENT PROGRESS IN RESIDUAL STRESS MEASUREMENT TECHNIQUES显示文摘Residual stress measurement is of critical significance to in-service security and the reliability of engineering components,and has been an active area of scientific interest.This paper ofers a review of several prominent mechanical release methods for residual stress measurement and recent developments,focusing on the hole-drilling method combined with advanced optical sensing.Some promising trends for mechanical release methods are also analyzed. | Xianfu Huang Zhanwei Liu Huimin Xie | 2013 | Acta Mechanica Solida Sinica2013，26，6： | 11 |
| 8 | A Discussion on the Origin of Shale Reservoir Inter-Laminar Fractures in the Shahejie Formation of Paleogene, Dongying Depression显示文摘This paper was conducted on the shale reservoir in the Dongying depression in the Shahejie Formation of Paleogene. Based on detailed core description, rock thin sections, argon ion polishing, scanning electron microscopy(SEM) analysis, CT scanning and carbon-oxygen isotopic test, the formation mechanism of the inter-laminar fractures(or seams) and their development conditions were discussed by comprehensive analysis of the diagenetic evolution features and the reservoir space evolution characteristics. The results show that the laminated composite pattern in Dongying depression was dominated by vertical distribution of laminated calcite and clay minerals. Contrasted to the traditional understanding, development degree of inter-laminar fractures was much lower. Pure fluid between layers cannot exist without framework minerals, and the pre-existing well connected pore or horizontal overpressure micro seam was favorable paths of fluid migration. From the points of inter-laminar fractures origin mechanism and its evolution, the so called seams, were much more complex than traditional understanding that hydrocarbon generation raised the pore pressure and led to the parallel microfractures. But the inter-laminar fractures had little relationship with that whether the lamination was developed or bedding boundary was clear or not. In fact, the shale reservoir inter-laminar fractures were not rigorous fracture. They were controlled by pre-existing inter-granular pore(or seam) or dissolved pore, which distributed along carbonate laminae boundary and were connected by later super pressure, dissolution and the seepage force. And the development conditions were burial depth(bigger than 3 000 m) and the Ro value(>0.6%). Discussion on its origin and evolution has important petroleum geological significance on optimizing reservoir segment and favorable target areas selection. | Huimin Liu Shun Zhang Guoqi Song Shoupeng Zhang Xuefeng Hao Zhonghuai Xie Ningning Xu Peng Liu | 2017 | Journal of Earth Science2017，28，6： | 10 |
| 9 | THE COMPLEXITY OF LIMIT LANGUAGES OF CELLULAR AUTOMATA: AN EXAMPLE显示文摘The limit inguages of cellular automata are defined and their complexity are discussed. New tools, which include skew evolution, skew periodic string, trace string, some algebraic calculation method, and restricted membership problem, are developed through a discussion focusing on the limit language of an elementary cellular automata of rule 94. It is proved that this language is non-regular. | XIE Huimin (Department of Mathematics, Suzhou University, Suzhou 215006, China) | 2001 | Journal of Systems Science & Complexity2001，14，1： | 8 |
| 10 | Electrochemically enhanced adsorption of PFOA and PFOS on multiwalled carbon nanotubes in continuous flow mode显示文摘It is important to develop efficient technologies on removal of perfluorooctanoic acid(PFOA)and perfluorooctane sulfonate(PFOS)from water due to their wide distribution and potential threat to human health.In this work,a durable and convenient electrosorption device was designed in continuous flow mode to investigate the adsorption of PFOX(X=A and S)on multiwalled carbon nanotubes(MWNTs)from water under electrochemical assistance.The electrosorption experiments were conducted under different influent and electrolyte concentrations,hydraulic retention time(HRT)and electrode distance to optimize the operation.The results showed that the highest removal efficiencies toward both PFOA and PFOS could come up to 90%at 1 V.Compared with open circuit(OC)adsorption under the same conditions,the removal efficiencies were improved by 4.9 times(PFOA)and 4.2 times(PFOS)respectively.In addition,the MWNTs electrode was found to be reusable.These findings provide an efficient method to remove PFOX from water by electrosorption in continuous flow mode. | Shuangyu Wang Xiaona Li Yaobin Zhang Xie Quan Shuo Chen Hongtao Yu Huimin Zhao | 2014 | Chinese Science Bulletin2014，59，23： | 8 |
| 11 | Fabrication technique of micro/nano-scale speckle patterns with focused ion beam显示文摘The fabrication technique of micro/nano-scale speckle patterns with focused ion beam (FIB) system is studied for digital image correlation (DIC) measurement under a scanning electron microscope (SEM).The speckle patterns are fabricated by directly etching the counterpart of the specimen to the black part of a template.Mean intensity gradient is used to evaluate the quality of these SEM images of speckle patterns fabricated based on different templates to select an optimum template.The pattern size depending on the displacement measurement sensitivity is adjusted by altering the magnification of FIB according to the relation curve of the etching size versus magnification.The influencing factors including etching time and ion beam current are discussed.Rigid body translation tests and rotation tests are carried out under SEM to verify the reliability of the fabricated speckle patterns.The calculated values are in good agreement with the imposed ones. | LI YanJie XIE HuiMin LUO Qiang GU ChangZhi HU ZhenXing CHEN PengWan ZHANG QingMing | 2012 | Science China(Physics,Mechanics & Astronomy)2012，55，6： | 7 |
| 12 | Synergistic therapy of magnetism-responsive hydrogel for soft tissue injuries显示文摘Soft tissue injury is very common and associated with pain,tissue swelling and even malformation if not treated on time.Treating methods include cryotherapy,electrical therapy,ultrasound therapy and anti-inflammatory drug,but none of them is completely satisfying.In this work,for a better therapeutic effect,drug therapy and pulsed electromagnetic field(PEMF)therapy were combined.We constructed a drug delivery system using the tetra-PEG/agar hydrogel(PA).By incorporating Fe3O4 NPs into the hydrogel network,a magnetism-responsive property was achieved in the system.The cytotoxicity and in vivo study showed a good biocompatibility of the PA/Fe3O4 hydrogel.A magnetism-controlled release was attained by the incorporation of Fe3O4.Finally,in vivo study showed a better performance of the DS-loaded PA/Fe3O4 compared with the commercially available DS ointment regarding the recovery of the injured soft tissue.Therefore,this magnetism-responsive hydrogel may represent a promising alternative to treat soft tissue injury. | Lining Zhang Xiuqin Zuo Shengjie Li Mi Sun Huimin Xie Kai Zhang Jikun Zhou Liyun Che Junxuan Ma Zishan Jia Fei Yang | 2019 | Bioactive Materials2019，4，1： | 7 |
| 13 | A micro-scale strain rosette for residual stress measurement by SEM Moiré method显示文摘In this paper,a new method combining focused ion beam(FIB)and scanning electron microscope(SEM)Moirétechnique for the measurement of residual stress at micro scale is proposed.The FIB is employed to introduce stress relief like the macro ring-core method and fabricate gratings with a frequency of 5000 lines/mm on the measured area of the sample surface.Three groups of gratings in different radial directions are manufactured in order to form a micro-scale strain rosette.After milling ring-core by FIB,the deformation incurred by relief of the stress will be recorded with the strain rosette.The displacement/strain field can be measured using SEM scanning Moiréwith random phase-shifting algorithm.In this study,the Nickel alloy GH4169 sample(which was processed by laser shock peening)is selected as a study object to determine its residual stress.The results showed that the components of the in-plane principal stresses were-359 MPa and-207 MPa,respectively,which show good agreement with the results obtained from the available literature. | ZHU RongHua XIE HuiMin ZHU JianGuo LI YanJie CHE ZhiGang ZOU ShiKun | 2014 | Science China(Physics,Mechanics & Astronomy)2014，57，4： | 6 |
| 14 | Spatial heterogeneity and source apportionment of soil metal(loid)s in an abandoned lead/zinc smelter显示文摘Metal smelting have brought severe metal(loid)s contamination to the soil.Spatial distribution and pollution source analysis for soil metal(loid)s in an abandoned lead/zinc smelter were studied.The results showed that soil was contaminated heavily withmetal(loid)s.The mean of lead(Pb),arsenic(As),cadmium(Cd),mercury(Hg)and antimony(Sb)content in topsoil is 9.7,8.2,5.0,2.3,and 1.2 times higher than the risk screening value for soil contamination of development land of China(GB36600-2018),respectively.Cd ismainly enriched in the 0–6mdepth of site soil while As and Pbmainly deposited in the 0–4mlayer.The spatial distribution of soil metal(loid)s is significantly correlated with the pollution source in the different functional areas of smelter.As,Hg,Sb,Pb and copper(Cu)were mainly distributed in pyrometallurgical area,while Cd,thallium(Tl)and zinc(Zn)was mainly existed in both hydrometallurgical area and raw material storage area.Soil metal(loid)s pollution sources in the abandoned smelter are mainly contributed to the anthropogenic sources,accounting for 84.5%.Specifically,Pb,Tl,As,Hg,Sb and Cumainly from atmospheric deposition(55.9%),Cd and Zn mainly from surface runoff(28.6%),While nickel(Ni)mainly comes from parent material(15.5%).The results clarified the spatial distribution and their sources in different functional areas of the smelter,providing a new thought for the risk prevention and control of metal(loid)s in polluted site soil. | Yunxia Zhang Tianshuang Li Zhaohui Guo Huimin Xie Zhihao Hu Hongzhen Ran Changzhou Li Zhichao Jiang | 2023 | Journal of Environmental Sciences2023，，5： | 5 |
| 15 | Identification of the elastic stiffness of composites using the virtual fields method and digital image correlation显示文摘This paper presents an effective methodology for characterizing the mechanical parameters of composites using digital image correlation combined with the virtual fields method.By using a three-point bending test configuration,this method can identify all mechanical parameters of the material with merely a single test.Successful results verified that this method is especially effective for characterizing composite materials.In this study,the method is applied to measure the orthotropic elastic parameters of fiber-reinforced polymer-matrix composites before and after the hygrothermal aging process.The results indicate that the hygrothermal aging environment significantly influences the mechanical property of a composite.The components of the parameters in the direction of the fiber bundle decreased significantly.From the accuracy analysis,we found that the actual measurement accuracy is sensitive to a shift of the horizontal edges and rotation of the vertical edges. | Lebin Jiang Baoqiao Guo Huimin Xie | 2015 | Acta Mechanica Sinica2015，31，2： | 5 |
| 16 | Bi-prism-based single-lens three dimensional digital image correlation system with a long working distance: Methodology and application in extreme high temperature deformation test显示文摘As a novel three dimensional digital image correlation(3 D DIC) method, the bi-prism-based single lens(BSL) 3 D DIC method has been proposed and developed in recent years. Making use of a bi-prism, this method is able to perform a 3 D DIC measurement using only a single camera. Thus, the integration level of a BSL 3 D DIC system could be much higher than that of the double-camera3 D DIC system. In this paper, using a small-angle bi-prism and a camera with a longer focal length, a special BSL 3 D DIC system with a long working distance is designed for measurements in extreme environments. The principle of the system is first studied,and practical methods are then proposed for the system set-up and the determination of system parameters. Then, feasibility of the measurement system is verified by out-of-plane rigid-body translation tests. Finally, the BSL 3 D DIC system is proven to be capable of combining with a high-temperature testing instrument to perform deformation tests in a high-temperature environment of up to 1500°C. | WU LiFu YIN YuanJie ZHANG Qi FANG DaiNing ZHANG RuBing ZHU JianGuo XIE HuiMin | 2018 | Science China(Technological Sciences)2018，61，1： | 5 |
| 17 | Electrocatalytic dechlorination of 2,4,5-trichlorobiphenyl using an aligned carbon nanotubes electrode deposited with palladium nanoparticles显示文摘Palladium loaded carbon nanotubes cathode with well-aligned nanotubes array was successfully fabricated on a titanium foil (Pd/CNTs/Ti) using a chemical vapor deposition technique and subsequent electrochemical deposition method. Pd particles were well dispersed on CNTs wall surfaces with average sizes no more than 20 nm, in most cases around 10 nm. Experiments for dechlorination of 2,4,5-trichlorobiphenyl (PCB 29) in methanol/water solution were carried out for the first time using Pd/CNTs/Ti cathode for investigation of its performance in electrocatalytic dechlorination of PCBs. Results show that Pd/CNTs/Ti presented better dechlorination efficiency (up to 90% in 6 h) than Pd/Ti and Pd/graphite cathodes owing to unique properties owned by CNTs, which benefited enhanced dechlorination of PCB 29. Complete dechlorination for PCB 29 was observed and biphenyl was identified to be final dechlorination product. The amount of Pd loading, cathode potential, and electrolytes were found to be key factors influencing dechlorination performance. | CHEN Shuo QIN ZhenLin QUAN Xie ZHANG YaoBin ZHAO HuiMin | 2010 | Chinese Science Bulletin2010，55，4： | 4 |
| 18 | Kinetics of enhanced adsorption by polarization for organic pollutants on activated carbon fiber显示文摘The adsorption kinetics for model pollutants on activated carbon fiber(ACF)by polarization was investigated in this work.Kinetics data obtained for the adsorption of these model pollutants at open-circuit,400 mV,and−400 mV polarization were applied to the Lagergren equation,and adsorption rate constants(Ka)were determined.With the anodic polarization of 400 mV,the capacity of sodium phenoxide was increased from 0.0083 mmol/g at open-circuit to 0.18 mmol/g,and a 17-fold enhancement was achieved;however,the capacity of p-nitrophenol was decreased from 2.93 mmol/g at open-circuit to 2.65 mmol/g.With the cathodal polarization of−400 mV,the capacity of aniline was improved from 3.60 mmol/g at open-circuit to 3.88 mmol/g;however,the capacity of sodium dodecylben-zene sulfonate was reduced from 2.20 mmol/g at open-circuit to 1.59 mmol/g.The enhancement for electrosorption changed with dif ferent groups substituting.Anodic polarization enhances the adsorption of benzene with the electron-donating group.But whether anodic or not,cathodal polariza-tion had less effect on the adsorption of electron-accepting aromatic compounds,and decreased the adsorption capacity of benzene-bearing donor-conjugate bridge-acceptor,while increasing its adsorption rate.Electrostatic interaction played a very important role in the electrosorption of ion-pollutants. | HAN Yanhe QUAN Xie ZHAO Huimin CHEN Shuo ZHAO Yazhi | 2007 | Frontiers of Environmental Science & Engineering2007，1，1： | 4 |
| 19 | Spatial distribution of IL4 controls iNKT cell-DC crosstalk in tumors显示文摘The spatiotemporal distribution of cytokines orchestrates immune responses in vivo,yet the underlying mechanisms remain to be explored.We showed here that the spatial distribution of interleukin-4(IL4)in invariant natural killer T(iNKT)cells regulated crosstalk between iNKT cells and dendritic cells(DCs)and controlled iNKT cell-mediated T-helper type 1(Th1)responses.The persistent polarization of IL4 induced by strong lipid antigens,that is,α-galactosylceramide(αGC),caused IL4 accumulation at the immunological synapse(IS),which promoted the activation of the IL4R-STAT6(signal transducer and activator of transcription 6)pathway and production of IL12 in DCs,which enhanced interferon-γ(IFNγ)production in iNKT cells.Conversely,the nonpolarized secretion of IL4 induced by Th2 lipid antigens with a short or unsaturated chain was incapable of enhancing this iNKT cell-DC crosstalk and thus shifted the immune response to a Th2-type response.The nonpolarized secretion of IL4 in response to Th2 lipid antigens was caused by the degradation of Cdc42 in iNKT cells.Moreover,reduced Cdc42 expression was observed in tumorinfiltrating iNKT cells,which impaired IL4 polarization and disturbed iNKT cell-DC crosstalk in tumors. | Lu Wang Zhilan Liu Lili Wang Qielan Wu Xiang Li Di Xie Huimin Zhang Yongdeng Zhang Lusheng Gu Yanhong Xue Ting Yue Gang Liu Wei Ji Haiming Wei Tao Xu Li Bai | 2020 | Cellular & Molecular Immunology2020，17，5： | 4 |
| 20 | In situ SEM-DIC technique and its application to characterize the high-temperature fatigue crack closure effect显示文摘In situ high-temperature(maximum: 650℃) experiments for fatigue crack growth on single edge-notched GH4169 superalloy specimens have been performed in scanning electron microscopy(SEM). In order to investigate the crack closure behavior,digital image correlation(DIC) method was applied to measure the full-field displacement and strain fields around the crack tip.The deformation carrier(speckle) was fabricated on the polished specimen surface with Zr O2 powders having a good hightemperature resistance, and the speckle patterns were recorded during the fatigue test by SEM. In consideration of the distortion of SEM images, the unabridged model and the bicubic model were used to correct the spatial distortion, and the distortion parameters can be determined by a calibration test. It is shown that the unabridged model makes a better contribution towards improving SEM-DIC measurement accuracy. Based on the deformation field, the mode Ι stress intensity factor range ?K and the crack opening displacement(COD) can be calculated for evaluating the crack closure effect. Additionally, the crack propagation was monitored using SEM and optical microscope. It indicates that the cracks grew initially in trans-granular mode at room temperature and 650°C, then propagated in both trans-granular and inter-granular modes. | YIN YuanJie XIE HuiMin HE Wei | 2020 | Science China(Technological Sciences)2020，63，2： | 4 |
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